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Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide
In the title compound, C(21)H(17)N(3)O(3)S, the non-H atoms, apart from those in the benzoyl group, are almost coplanar (r.m.s. deviation = 0.049 Å) and the benzoyl group is almost orthogonal to the plane of the rest of the molecule [dihedral angle = 80.34 (6)°]. In the crystal, a combination of N—...
| Autores principales: | , , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2016
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4971849/ https://www.ncbi.nlm.nih.gov/pubmed/27536390 http://dx.doi.org/10.1107/S2056989016010975 |
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| author | Subbulakshmi, Karanth N. Narayana, Badiadka Yathirajan, Hemmige S. Jasinski, Jerry P. Rathore, Ravindranath S. Glidewell, Christopher |
| author_facet | Subbulakshmi, Karanth N. Narayana, Badiadka Yathirajan, Hemmige S. Jasinski, Jerry P. Rathore, Ravindranath S. Glidewell, Christopher |
| author_sort | Subbulakshmi, Karanth N. |
| collection | PubMed |
| description | In the title compound, C(21)H(17)N(3)O(3)S, the non-H atoms, apart from those in the benzoyl group, are almost coplanar (r.m.s. deviation = 0.049 Å) and the benzoyl group is almost orthogonal to the plane of the rest of the molecule [dihedral angle = 80.34 (6)°]. In the crystal, a combination of N—H⋯O and asymmetric bifurcated O—H⋯(N,O) hydrogen bonds link the molecules into a three-dimensional network. Weak C—H⋯O interactions are also observed. |
| format | Online Article Text |
| id | pubmed-4971849 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2016 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-49718492016-08-17 Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide Subbulakshmi, Karanth N. Narayana, Badiadka Yathirajan, Hemmige S. Jasinski, Jerry P. Rathore, Ravindranath S. Glidewell, Christopher Acta Crystallogr E Crystallogr Commun Research Communications In the title compound, C(21)H(17)N(3)O(3)S, the non-H atoms, apart from those in the benzoyl group, are almost coplanar (r.m.s. deviation = 0.049 Å) and the benzoyl group is almost orthogonal to the plane of the rest of the molecule [dihedral angle = 80.34 (6)°]. In the crystal, a combination of N—H⋯O and asymmetric bifurcated O—H⋯(N,O) hydrogen bonds link the molecules into a three-dimensional network. Weak C—H⋯O interactions are also observed. International Union of Crystallography 2016-07-12 /pmc/articles/PMC4971849/ /pubmed/27536390 http://dx.doi.org/10.1107/S2056989016010975 Text en © Subbulakshmi et al. 2016 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Research Communications Subbulakshmi, Karanth N. Narayana, Badiadka Yathirajan, Hemmige S. Jasinski, Jerry P. Rathore, Ravindranath S. Glidewell, Christopher Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| title | Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| title_full | Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| title_fullStr | Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| title_full_unstemmed | Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| title_short | Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| title_sort | crystal structure of 2-benzoylamino-n′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide |
| topic | Research Communications |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4971849/ https://www.ncbi.nlm.nih.gov/pubmed/27536390 http://dx.doi.org/10.1107/S2056989016010975 |
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