Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one

In the title compound, C(15)H(12)N(4)O(4), the dihedral angle between the heterocyclic rings is 12.60 (8)°, and that between the benzene ring and the adjacent heterocyclic ring is 85.14 (6)°. In the crystal, a combination of N—H⋯O and O—H⋯O hydrogen bonds link mol­ecules related by a glide plane int...

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Autores principales: Sagar, Belakavadi K., Yathirajan, Hemmige S., Jasinski, Jerry P., Glidewell, Christopher
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2016
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4992917/
https://www.ncbi.nlm.nih.gov/pubmed/27555942
http://dx.doi.org/10.1107/S2056989016009075
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author Sagar, Belakavadi K.
Yathirajan, Hemmige S.
Jasinski, Jerry P.
Glidewell, Christopher
author_facet Sagar, Belakavadi K.
Yathirajan, Hemmige S.
Jasinski, Jerry P.
Glidewell, Christopher
author_sort Sagar, Belakavadi K.
collection PubMed
description In the title compound, C(15)H(12)N(4)O(4), the dihedral angle between the heterocyclic rings is 12.60 (8)°, and that between the benzene ring and the adjacent heterocyclic ring is 85.14 (6)°. In the crystal, a combination of N—H⋯O and O—H⋯O hydrogen bonds link mol­ecules related by a glide plane into a C(5) C(6)[R (2) (2)(9)] chain of rings, which is a distinctly different packing motif to those observed in hydrated modifications of this compound.
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spelling pubmed-49929172016-08-23 Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one Sagar, Belakavadi K. Yathirajan, Hemmige S. Jasinski, Jerry P. Glidewell, Christopher Acta Crystallogr E Crystallogr Commun Research Communications In the title compound, C(15)H(12)N(4)O(4), the dihedral angle between the heterocyclic rings is 12.60 (8)°, and that between the benzene ring and the adjacent heterocyclic ring is 85.14 (6)°. In the crystal, a combination of N—H⋯O and O—H⋯O hydrogen bonds link mol­ecules related by a glide plane into a C(5) C(6)[R (2) (2)(9)] chain of rings, which is a distinctly different packing motif to those observed in hydrated modifications of this compound. International Union of Crystallography 2016-06-17 /pmc/articles/PMC4992917/ /pubmed/27555942 http://dx.doi.org/10.1107/S2056989016009075 Text en © Sagar et al. 2016 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Sagar, Belakavadi K.
Yathirajan, Hemmige S.
Jasinski, Jerry P.
Glidewell, Christopher
Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one
title Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one
title_full Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one
title_fullStr Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one
title_full_unstemmed Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one
title_short Crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3H)-one
title_sort crystal structure of 6-hy­droxy-5-(2-meth­oxy­phenoxy)-2,2′-bipyrimidin-4(3h)-one
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4992917/
https://www.ncbi.nlm.nih.gov/pubmed/27555942
http://dx.doi.org/10.1107/S2056989016009075
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