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High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach

We have demonstrated the synthesis of γ-Fe(2)O(3) nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-parti...

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Detalles Bibliográficos
Autores principales: Cao, Derang, Li, Hao, Pan, Lining, Li, Jianan, Wang, Xicheng, Jing, Panpan, Cheng, Xiaohong, Wang, Wenjie, Wang, Jianbo, Liu, Qingfang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group 2016
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5007676/
https://www.ncbi.nlm.nih.gov/pubmed/27581732
http://dx.doi.org/10.1038/srep32360
Descripción
Sumario:We have demonstrated the synthesis of γ-Fe(2)O(3) nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-particles is proposed, and DMF as a polar solvent may slower the reaction process of calcination. The structures, morphologies, and magnetic properties of γ-Fe(2)O(3) nano-particles were investigated systematically, and the pure γ-Fe(2)O(3) nano-particles obtained at 200 °C display uniform morphology good magnetic property. The saturation magnetization of obtained pure γ-Fe(2)O(3) is about 74 emu/g, which is comparable with bulk material (76 emu/g) and larger than other results. In addition, the photocatalytic activity for degradation of methylene blue is also studied, which shows proper photocatalytic activity.