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High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach

We have demonstrated the synthesis of γ-Fe(2)O(3) nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-parti...

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Autores principales: Cao, Derang, Li, Hao, Pan, Lining, Li, Jianan, Wang, Xicheng, Jing, Panpan, Cheng, Xiaohong, Wang, Wenjie, Wang, Jianbo, Liu, Qingfang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group 2016
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5007676/
https://www.ncbi.nlm.nih.gov/pubmed/27581732
http://dx.doi.org/10.1038/srep32360
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author Cao, Derang
Li, Hao
Pan, Lining
Li, Jianan
Wang, Xicheng
Jing, Panpan
Cheng, Xiaohong
Wang, Wenjie
Wang, Jianbo
Liu, Qingfang
author_facet Cao, Derang
Li, Hao
Pan, Lining
Li, Jianan
Wang, Xicheng
Jing, Panpan
Cheng, Xiaohong
Wang, Wenjie
Wang, Jianbo
Liu, Qingfang
author_sort Cao, Derang
collection PubMed
description We have demonstrated the synthesis of γ-Fe(2)O(3) nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-particles is proposed, and DMF as a polar solvent may slower the reaction process of calcination. The structures, morphologies, and magnetic properties of γ-Fe(2)O(3) nano-particles were investigated systematically, and the pure γ-Fe(2)O(3) nano-particles obtained at 200 °C display uniform morphology good magnetic property. The saturation magnetization of obtained pure γ-Fe(2)O(3) is about 74 emu/g, which is comparable with bulk material (76 emu/g) and larger than other results. In addition, the photocatalytic activity for degradation of methylene blue is also studied, which shows proper photocatalytic activity.
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spelling pubmed-50076762016-09-08 High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach Cao, Derang Li, Hao Pan, Lining Li, Jianan Wang, Xicheng Jing, Panpan Cheng, Xiaohong Wang, Wenjie Wang, Jianbo Liu, Qingfang Sci Rep Article We have demonstrated the synthesis of γ-Fe(2)O(3) nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-particles is proposed, and DMF as a polar solvent may slower the reaction process of calcination. The structures, morphologies, and magnetic properties of γ-Fe(2)O(3) nano-particles were investigated systematically, and the pure γ-Fe(2)O(3) nano-particles obtained at 200 °C display uniform morphology good magnetic property. The saturation magnetization of obtained pure γ-Fe(2)O(3) is about 74 emu/g, which is comparable with bulk material (76 emu/g) and larger than other results. In addition, the photocatalytic activity for degradation of methylene blue is also studied, which shows proper photocatalytic activity. Nature Publishing Group 2016-09-01 /pmc/articles/PMC5007676/ /pubmed/27581732 http://dx.doi.org/10.1038/srep32360 Text en Copyright © 2016, The Author(s) http://creativecommons.org/licenses/by/4.0/ This work is licensed under a Creative Commons Attribution 4.0 International License. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in the credit line; if the material is not included under the Creative Commons license, users will need to obtain permission from the license holder to reproduce the material. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/
spellingShingle Article
Cao, Derang
Li, Hao
Pan, Lining
Li, Jianan
Wang, Xicheng
Jing, Panpan
Cheng, Xiaohong
Wang, Wenjie
Wang, Jianbo
Liu, Qingfang
High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach
title High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach
title_full High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach
title_fullStr High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach
title_full_unstemmed High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach
title_short High saturation magnetization of γ-Fe(2)O(3) nano-particles by a facile one-step synthesis approach
title_sort high saturation magnetization of γ-fe(2)o(3) nano-particles by a facile one-step synthesis approach
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5007676/
https://www.ncbi.nlm.nih.gov/pubmed/27581732
http://dx.doi.org/10.1038/srep32360
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