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Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS
The Extended Q-range Small-angle Neutron Scattering Diffractometer (EQ-SANS) instrument at the spallation neutron source (SNS), Oak Ridge, Tennessee, incorporates a 69 m(3) detector vessel with a vacuum system which required an upgrade with respect to performance, ease of operation, and maintenance....
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2016
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5065636/ https://www.ncbi.nlm.nih.gov/pubmed/27766212 http://dx.doi.org/10.1016/j.mex.2016.09.002 |
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author | Stone, Christopher Williams, Derrick Price, Jeremy |
author_facet | Stone, Christopher Williams, Derrick Price, Jeremy |
author_sort | Stone, Christopher |
collection | PubMed |
description | The Extended Q-range Small-angle Neutron Scattering Diffractometer (EQ-SANS) instrument at the spallation neutron source (SNS), Oak Ridge, Tennessee, incorporates a 69 m(3) detector vessel with a vacuum system which required an upgrade with respect to performance, ease of operation, and maintenance. The upgrade focused on improving pumping performance as well as optimizing system design to minimize opportunity for operational error. This upgrade provided the following practical contributions: • Reduced time required to evacuate from atmospheric pressure to 2 mTorr from 500 to 1000 min to 60–70 min; • Provided turn-key automated control with a multi-faceted interlock for personnel and machine safety. |
format | Online Article Text |
id | pubmed-5065636 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2016 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-50656362016-10-20 Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS Stone, Christopher Williams, Derrick Price, Jeremy MethodsX Engineering The Extended Q-range Small-angle Neutron Scattering Diffractometer (EQ-SANS) instrument at the spallation neutron source (SNS), Oak Ridge, Tennessee, incorporates a 69 m(3) detector vessel with a vacuum system which required an upgrade with respect to performance, ease of operation, and maintenance. The upgrade focused on improving pumping performance as well as optimizing system design to minimize opportunity for operational error. This upgrade provided the following practical contributions: • Reduced time required to evacuate from atmospheric pressure to 2 mTorr from 500 to 1000 min to 60–70 min; • Provided turn-key automated control with a multi-faceted interlock for personnel and machine safety. Elsevier 2016-09-23 /pmc/articles/PMC5065636/ /pubmed/27766212 http://dx.doi.org/10.1016/j.mex.2016.09.002 Text en © 2016 The Author(s) http://creativecommons.org/licenses/by-nc-nd/4.0/ This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). |
spellingShingle | Engineering Stone, Christopher Williams, Derrick Price, Jeremy Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS |
title | Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS |
title_full | Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS |
title_fullStr | Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS |
title_full_unstemmed | Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS |
title_short | Vacuum system upgrade for extended Q-range small-angle neutron scattering diffractometer (EQ-SANS) at SNS |
title_sort | vacuum system upgrade for extended q-range small-angle neutron scattering diffractometer (eq-sans) at sns |
topic | Engineering |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5065636/ https://www.ncbi.nlm.nih.gov/pubmed/27766212 http://dx.doi.org/10.1016/j.mex.2016.09.002 |
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