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Mechanochemical synthesis and crystal structure of a 1:2 co-crystal of 1,3,6,8-tetra­aza­tri­cyclo[4.3.1.1(3,8)]undecane (TATU) and 4-chloro-3,5-dimethyl­phenol

Solvent-free treatment of 1,3,6,8-tetra­aza­tri­cyclo­[4.3.1.1(3,8)]undecano (TATU) with 4-chloro-3,5-di­methyl­phenol led to the formation of the title co-crystal, C(7)H(14)N(4)·2C(8)H(9)ClO. The asymmetric unit contains one aminal cage mol­ecule and two phenol mol­ecules linked via two O—H⋯N hydro...

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Detalles Bibliográficos
Autores principales: Rivera, Augusto, Rojas, Jicli José, Sadat-Bernal, John, Ríos-Motta, Jaime, Bolte, Michael
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2016
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5095854/
https://www.ncbi.nlm.nih.gov/pubmed/27840729
http://dx.doi.org/10.1107/S2056989016016650