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Mechanochemical synthesis and crystal structure of a 1:2 co-crystal of 1,3,6,8-tetraazatricyclo[4.3.1.1(3,8)]undecane (TATU) and 4-chloro-3,5-dimethylphenol
Solvent-free treatment of 1,3,6,8-tetraazatricyclo[4.3.1.1(3,8)]undecano (TATU) with 4-chloro-3,5-dimethylphenol led to the formation of the title co-crystal, C(7)H(14)N(4)·2C(8)H(9)ClO. The asymmetric unit contains one aminal cage molecule and two phenol molecules linked via two O—H⋯N hydro...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2016
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5095854/ https://www.ncbi.nlm.nih.gov/pubmed/27840729 http://dx.doi.org/10.1107/S2056989016016650 |