Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole

The title compound, C(12)H(15)NO(3)S, was prepared by 1,3-dipolar cyclo­addition of 3,4-di­hydro-2H-pyrrole 1-oxide and phenyl vinyl sulfone. In the mol­ecule, both fused five-membered rings display a twisted conformation. In the crystal, C—H⋯O hydrogen bonds link neighbouring mol­ecules, forming ch...

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Autores principales: Hernández, Yaiza, Marcos, Isidro, Garrido, Narciso M., Sanz, Francisca, Diez, David
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2017
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5209779/
https://www.ncbi.nlm.nih.gov/pubmed/28083143
http://dx.doi.org/10.1107/S2056989016019952
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author Hernández, Yaiza
Marcos, Isidro
Garrido, Narciso M.
Sanz, Francisca
Diez, David
author_facet Hernández, Yaiza
Marcos, Isidro
Garrido, Narciso M.
Sanz, Francisca
Diez, David
author_sort Hernández, Yaiza
collection PubMed
description The title compound, C(12)H(15)NO(3)S, was prepared by 1,3-dipolar cyclo­addition of 3,4-di­hydro-2H-pyrrole 1-oxide and phenyl vinyl sulfone. In the mol­ecule, both fused five-membered rings display a twisted conformation. In the crystal, C—H⋯O hydrogen bonds link neighbouring mol­ecules, forming chains running parallel to the b axis.
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spelling pubmed-52097792017-01-12 Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole Hernández, Yaiza Marcos, Isidro Garrido, Narciso M. Sanz, Francisca Diez, David Acta Crystallogr E Crystallogr Commun Research Communications The title compound, C(12)H(15)NO(3)S, was prepared by 1,3-dipolar cyclo­addition of 3,4-di­hydro-2H-pyrrole 1-oxide and phenyl vinyl sulfone. In the mol­ecule, both fused five-membered rings display a twisted conformation. In the crystal, C—H⋯O hydrogen bonds link neighbouring mol­ecules, forming chains running parallel to the b axis. International Union of Crystallography 2017-01-01 /pmc/articles/PMC5209779/ /pubmed/28083143 http://dx.doi.org/10.1107/S2056989016019952 Text en © Hernández et al. 2017 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Hernández, Yaiza
Marcos, Isidro
Garrido, Narciso M.
Sanz, Francisca
Diez, David
Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
title Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
title_full Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
title_fullStr Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
title_full_unstemmed Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
title_short Crystal structure of (2R*,3aR*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
title_sort crystal structure of (2r*,3ar*)-2-phenyl­sulfonyl-2,3,3a,4,5,6-hexa­hydro­pyrrolo­[1,2-b]isoxazole
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5209779/
https://www.ncbi.nlm.nih.gov/pubmed/28083143
http://dx.doi.org/10.1107/S2056989016019952
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