Characterization of the synthetic cannabinoid MDMB-CHMCZCA

The synthetic cannabinoid MDMB-CHMCZCA was characterized by various spectroscopic techniques including NMR spectroscopy and tandem mass spectrometry. The synthetic sample was found to be of S-configuration by VCD spectroscopy and comparison of the data with DFT calculations, while ECD spectroscopy w...

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Detalles Bibliográficos
Autores principales: Weber, Carina, Pusch, Stefan, Schollmeyer, Dieter, Münster-Müller, Sascha, Pütz, Michael, Opatz, Till
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2016
Materias:
Full Research Paper
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5238538/
https://www.ncbi.nlm.nih.gov/pubmed/28144353
http://dx.doi.org/10.3762/bjoc.12.279
Descripción
Sumario:The synthetic cannabinoid MDMB-CHMCZCA was characterized by various spectroscopic techniques including NMR spectroscopy and tandem mass spectrometry. The synthetic sample was found to be of S-configuration by VCD spectroscopy and comparison of the data with DFT calculations, while ECD spectroscopy was found to be inconclusive in this case. The enantiomeric purity of samples from test purchases and police seizures was assessed by a self-developed chiral HPLC method.

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