Characterization of the synthetic cannabinoid MDMB-CHMCZCA

The synthetic cannabinoid MDMB-CHMCZCA was characterized by various spectroscopic techniques including NMR spectroscopy and tandem mass spectrometry. The synthetic sample was found to be of S-configuration by VCD spectroscopy and comparison of the data with DFT calculations, while ECD spectroscopy w...

Descripción completa

Detalles Bibliográficos
Autores principales: Weber, Carina, Pusch, Stefan, Schollmeyer, Dieter, Münster-Müller, Sascha, Pütz, Michael, Opatz, Till
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2016
Materias:
Full Research Paper
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5238538/
https://www.ncbi.nlm.nih.gov/pubmed/28144353
http://dx.doi.org/10.3762/bjoc.12.279
_version_ 1782495721314844672
author Weber, Carina
Pusch, Stefan
Schollmeyer, Dieter
Münster-Müller, Sascha
Pütz, Michael
Opatz, Till
author_facet Weber, Carina
Pusch, Stefan
Schollmeyer, Dieter
Münster-Müller, Sascha
Pütz, Michael
Opatz, Till
author_sort Weber, Carina
collection PubMed
description The synthetic cannabinoid MDMB-CHMCZCA was characterized by various spectroscopic techniques including NMR spectroscopy and tandem mass spectrometry. The synthetic sample was found to be of S-configuration by VCD spectroscopy and comparison of the data with DFT calculations, while ECD spectroscopy was found to be inconclusive in this case. The enantiomeric purity of samples from test purchases and police seizures was assessed by a self-developed chiral HPLC method.
format Online
Article
Text
id pubmed-5238538
institution National Center for Biotechnology Information
language English
publishDate 2016
publisher Beilstein-Institut
record_format MEDLINE/PubMed
spelling pubmed-52385382017-01-31 Characterization of the synthetic cannabinoid MDMB-CHMCZCA Weber, Carina Pusch, Stefan Schollmeyer, Dieter Münster-Müller, Sascha Pütz, Michael Opatz, Till Beilstein J Org Chem Full Research Paper The synthetic cannabinoid MDMB-CHMCZCA was characterized by various spectroscopic techniques including NMR spectroscopy and tandem mass spectrometry. The synthetic sample was found to be of S-configuration by VCD spectroscopy and comparison of the data with DFT calculations, while ECD spectroscopy was found to be inconclusive in this case. The enantiomeric purity of samples from test purchases and police seizures was assessed by a self-developed chiral HPLC method. Beilstein-Institut 2016-12-21 /pmc/articles/PMC5238538/ /pubmed/28144353 http://dx.doi.org/10.3762/bjoc.12.279 Text en Copyright © 2016, Weber et al. https://creativecommons.org/licenses/by/4.0https://www.beilstein-journals.org/bjoc/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (https://www.beilstein-journals.org/bjoc/terms)
spellingShingle Full Research Paper
Weber, Carina
Pusch, Stefan
Schollmeyer, Dieter
Münster-Müller, Sascha
Pütz, Michael
Opatz, Till
Characterization of the synthetic cannabinoid MDMB-CHMCZCA
title Characterization of the synthetic cannabinoid MDMB-CHMCZCA
title_full Characterization of the synthetic cannabinoid MDMB-CHMCZCA
title_fullStr Characterization of the synthetic cannabinoid MDMB-CHMCZCA
title_full_unstemmed Characterization of the synthetic cannabinoid MDMB-CHMCZCA
title_short Characterization of the synthetic cannabinoid MDMB-CHMCZCA
title_sort characterization of the synthetic cannabinoid mdmb-chmczca
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5238538/
https://www.ncbi.nlm.nih.gov/pubmed/28144353
http://dx.doi.org/10.3762/bjoc.12.279
work_keys_str_mv AT webercarina characterizationofthesyntheticcannabinoidmdmbchmczca
AT puschstefan characterizationofthesyntheticcannabinoidmdmbchmczca
AT schollmeyerdieter characterizationofthesyntheticcannabinoidmdmbchmczca
AT munstermullersascha characterizationofthesyntheticcannabinoidmdmbchmczca
AT putzmichael characterizationofthesyntheticcannabinoidmdmbchmczca
AT opatztill characterizationofthesyntheticcannabinoidmdmbchmczca

Ejemplares similares