Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys

A procedure is described for the determination of aluminum in high temperature alloys. Aluminum is selectively precipitated with 8-hydroxyquinoline from an ammoniacal solution of the alloy containing citrate and cyanide as complexing agents. The precipitate is ignited under oxalic acid, the oxides f...

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Detalles Bibliográficos
Autores principales: Machlan, Lawrence A., Hague, John L., Meros, Edward J.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: [Gaithersburg, MD] : U.S. Dept. of Commerce, National Institute of Standards and Technology 1960
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5287263/
https://www.ncbi.nlm.nih.gov/pubmed/32196223
http://dx.doi.org/10.6028/jres.064A.019
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author Machlan, Lawrence A.
Hague, John L.
Meros, Edward J.
author_facet Machlan, Lawrence A.
Hague, John L.
Meros, Edward J.
author_sort Machlan, Lawrence A.
collection PubMed
description A procedure is described for the determination of aluminum in high temperature alloys. Aluminum is selectively precipitated with 8-hydroxyquinoline from an ammoniacal solution of the alloy containing citrate and cyanide as complexing agents. The precipitate is ignited under oxalic acid, the oxides fused, and dissolved in acid. A caustic precipitation is made, an aliquot of the filtrate treated with hydrogen peroxide, and the aluminum precipitated with 8-hydroxyquinoline. The aluminum hydroxyquinolate is filtered on a fritted-glass crucible, dried, and weighed.
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spelling pubmed-52872632020-03-18 Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys Machlan, Lawrence A. Hague, John L. Meros, Edward J. J Res Natl Bur Stand A Phys Chem Article A procedure is described for the determination of aluminum in high temperature alloys. Aluminum is selectively precipitated with 8-hydroxyquinoline from an ammoniacal solution of the alloy containing citrate and cyanide as complexing agents. The precipitate is ignited under oxalic acid, the oxides fused, and dissolved in acid. A caustic precipitation is made, an aliquot of the filtrate treated with hydrogen peroxide, and the aluminum precipitated with 8-hydroxyquinoline. The aluminum hydroxyquinolate is filtered on a fritted-glass crucible, dried, and weighed. [Gaithersburg, MD] : U.S. Dept. of Commerce, National Institute of Standards and Technology 1960 1960-04-01 /pmc/articles/PMC5287263/ /pubmed/32196223 http://dx.doi.org/10.6028/jres.064A.019 Text en https://creativecommons.org/publicdomain/zero/1.0/ The Journal of Research of the National Bureau of Standards Section A is a publication of the U.S. Government. The papers are in the public domain and are not subject to copyright in the United States. Articles from J Res may contain photographs or illustrations copyrighted by other commercial organizations or individuals that may not be used without obtaining prior approval from the holder of the copyright.
spellingShingle Article
Machlan, Lawrence A.
Hague, John L.
Meros, Edward J.
Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys
title Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys
title_full Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys
title_fullStr Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys
title_full_unstemmed Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys
title_short Determination of Aluminum in Precipitation Hardening Stainless Steel and High Temperature Alloys
title_sort determination of aluminum in precipitation hardening stainless steel and high temperature alloys
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5287263/
https://www.ncbi.nlm.nih.gov/pubmed/32196223
http://dx.doi.org/10.6028/jres.064A.019
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AT haguejohnl determinationofaluminuminprecipitationhardeningstainlesssteelandhightemperaturealloys
AT merosedwardj determinationofaluminuminprecipitationhardeningstainlesssteelandhightemperaturealloys

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