Preparation of Anhydrous Single Crystals of Rare-Earth Halides

Anhydrous rare-earth halides are prepared by the conversion of the rare-earth oxide to the halide by means of its reaction with the appropriate ammonium halide. Without transfer from the reaction vessel, the halide is melted, then crystallized by slow cooling. The resulting solid usually contains si...

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Detalles Bibliográficos
Autor principal: Kiess, Norman H.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: [Gaithersburg, MD] : U.S. Dept. of Commerce, National Institute of Standards and Technology 1963
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5317228/
https://www.ncbi.nlm.nih.gov/pubmed/31580572
http://dx.doi.org/10.6028/jres.067A.036
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author Kiess, Norman H.
author_facet Kiess, Norman H.
author_sort Kiess, Norman H.
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description Anhydrous rare-earth halides are prepared by the conversion of the rare-earth oxide to the halide by means of its reaction with the appropriate ammonium halide. Without transfer from the reaction vessel, the halide is melted, then crystallized by slow cooling. The resulting solid usually contains single crystals large enough to permit spectroscopic studies of the compounds.
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spelling pubmed-53172282019-10-01 Preparation of Anhydrous Single Crystals of Rare-Earth Halides Kiess, Norman H. J Res Natl Bur Stand A Phys Chem Article Anhydrous rare-earth halides are prepared by the conversion of the rare-earth oxide to the halide by means of its reaction with the appropriate ammonium halide. Without transfer from the reaction vessel, the halide is melted, then crystallized by slow cooling. The resulting solid usually contains single crystals large enough to permit spectroscopic studies of the compounds. [Gaithersburg, MD] : U.S. Dept. of Commerce, National Institute of Standards and Technology 1963 1963-08-01 /pmc/articles/PMC5317228/ /pubmed/31580572 http://dx.doi.org/10.6028/jres.067A.036 Text en https://creativecommons.org/publicdomain/zero/1.0/ The Journal of Research of the National Bureau of Standards Section A is a publication of the U.S. Government. The papers are in the public domain and are not subject to copyright in the United States. Articles from J Res may contain photographs or illustrations copyrighted by other commercial organizations or individuals that may not be used without obtaining prior approval from the holder of the copyright.
spellingShingle Article
Kiess, Norman H.
Preparation of Anhydrous Single Crystals of Rare-Earth Halides
title Preparation of Anhydrous Single Crystals of Rare-Earth Halides
title_full Preparation of Anhydrous Single Crystals of Rare-Earth Halides
title_fullStr Preparation of Anhydrous Single Crystals of Rare-Earth Halides
title_full_unstemmed Preparation of Anhydrous Single Crystals of Rare-Earth Halides
title_short Preparation of Anhydrous Single Crystals of Rare-Earth Halides
title_sort preparation of anhydrous single crystals of rare-earth halides
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5317228/
https://www.ncbi.nlm.nih.gov/pubmed/31580572
http://dx.doi.org/10.6028/jres.067A.036
work_keys_str_mv AT kiessnormanh preparationofanhydroussinglecrystalsofrareearthhalides

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