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Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS

The chemical composition of sandarac resin was investigated qualitatively and quantitatively by gas chromatography-mass spectrometry (GC-MS). Six compounds with labdane and pimarane skeletons were identified in the resin. The obtained mass spectra were interpreted and the mass spectrometric behaviou...

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Autores principales: Kononenko, I., de Viguerie, L., Rochut, S., Walter, Ph.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer Berlin Heidelberg 2016
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5340847/
https://www.ncbi.nlm.nih.gov/pubmed/27464664
http://dx.doi.org/10.1007/s11356-016-7261-5
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author Kononenko, I.
de Viguerie, L.
Rochut, S.
Walter, Ph.
author_facet Kononenko, I.
de Viguerie, L.
Rochut, S.
Walter, Ph.
author_sort Kononenko, I.
collection PubMed
description The chemical composition of sandarac resin was investigated qualitatively and quantitatively by gas chromatography-mass spectrometry (GC-MS). Six compounds with labdane and pimarane skeletons were identified in the resin. The obtained mass spectra were interpreted and the mass spectrometric behaviour of these diterpenoids under EI conditions was described. Quantitative analysis by the method of internal standard revealed that identified diterpenoids represent only 10–30% of the analysed sample. The sandarac resin from different suppliers was analysed (from Kremer, Okhra, Color Rare, La Marchande de Couleurs, L'Atelier Montessori, Hevea). The analysis of different lumps of resins showed that the chemical composition differs from one lump to another, varying mainly in the relative distributions of the components.
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spelling pubmed-53408472017-03-20 Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS Kononenko, I. de Viguerie, L. Rochut, S. Walter, Ph. Environ Sci Pollut Res Int Art and Cultural Heritage The chemical composition of sandarac resin was investigated qualitatively and quantitatively by gas chromatography-mass spectrometry (GC-MS). Six compounds with labdane and pimarane skeletons were identified in the resin. The obtained mass spectra were interpreted and the mass spectrometric behaviour of these diterpenoids under EI conditions was described. Quantitative analysis by the method of internal standard revealed that identified diterpenoids represent only 10–30% of the analysed sample. The sandarac resin from different suppliers was analysed (from Kremer, Okhra, Color Rare, La Marchande de Couleurs, L'Atelier Montessori, Hevea). The analysis of different lumps of resins showed that the chemical composition differs from one lump to another, varying mainly in the relative distributions of the components. Springer Berlin Heidelberg 2016-07-28 2017 /pmc/articles/PMC5340847/ /pubmed/27464664 http://dx.doi.org/10.1007/s11356-016-7261-5 Text en © The Author(s) 2016 Open Access This article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.
spellingShingle Art and Cultural Heritage
Kononenko, I.
de Viguerie, L.
Rochut, S.
Walter, Ph.
Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS
title Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS
title_full Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS
title_fullStr Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS
title_full_unstemmed Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS
title_short Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS
title_sort qualitative and quantitative studies of chemical composition of sandarac resin by gc-ms
topic Art and Cultural Heritage
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5340847/
https://www.ncbi.nlm.nih.gov/pubmed/27464664
http://dx.doi.org/10.1007/s11356-016-7261-5
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