Influence of QuEChERS modifications on recovery and matrix effect during the multi-residue pesticide analysis in soil by GC/MS/MS and GC/ECD/NPD

A QuEChERS extraction followed by GC/MS/MS and GC-μECD/NPD for 216 pesticide and metabolites determination in soil simultaneously were developed and compared. Volume of water, volume and polarity of solvent, and cleanup sorbents (C18, GCB, PSA) were optimized. The QuEChERS with and without purificat...

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Detalles Bibliográficos
Autores principales: Łozowicka, Bożena, Rutkowska, Ewa, Jankowska, Magdalena
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer Berlin Heidelberg 2017
Materias:
Research Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5383684/
https://www.ncbi.nlm.nih.gov/pubmed/28093672
http://dx.doi.org/10.1007/s11356-016-8334-1

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5383684/
https://www.ncbi.nlm.nih.gov/pubmed/28093672
http://dx.doi.org/10.1007/s11356-016-8334-1

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