Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic

Bulk B-C-N materials were synthesized under static high thermobaric conditions (20 GPa and 2,000 °C) in a multianvil apparatus from a polymer derived t-BC(1.97)N ceramic. The bulk samples were characterised using X-ray synchrotron radiation and analytical transmission electron microscopy in combinat...

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Autores principales: Matizamhuka, Wallace R., Sigalas, Iakovos, Herrmann, Mathias, Dubronvinsky, Leonid, Dubrovinskaia, Natalia, Miyajima, Nobuyoshi, Mera, Gabriela, Riedel, Ralf
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2011
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5448883/
https://www.ncbi.nlm.nih.gov/pubmed/28824124
http://dx.doi.org/10.3390/ma4122061
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author Matizamhuka, Wallace R.
Sigalas, Iakovos
Herrmann, Mathias
Dubronvinsky, Leonid
Dubrovinskaia, Natalia
Miyajima, Nobuyoshi
Mera, Gabriela
Riedel, Ralf
author_facet Matizamhuka, Wallace R.
Sigalas, Iakovos
Herrmann, Mathias
Dubronvinsky, Leonid
Dubrovinskaia, Natalia
Miyajima, Nobuyoshi
Mera, Gabriela
Riedel, Ralf
author_sort Matizamhuka, Wallace R.
collection PubMed
description Bulk B-C-N materials were synthesized under static high thermobaric conditions (20 GPa and 2,000 °C) in a multianvil apparatus from a polymer derived t-BC(1.97)N ceramic. The bulk samples were characterised using X-ray synchrotron radiation and analytical transmission electron microscopy in combination with electron energy loss spectroscopy. Polycrystalline B-C-N materials with a cubic type structure were formed under the applied reaction conditions, but the formation of a ternary cubic diamond-like c-BC(2)N compound, could not be unambiguously confirmed.
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spelling pubmed-54488832017-07-28 Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic Matizamhuka, Wallace R. Sigalas, Iakovos Herrmann, Mathias Dubronvinsky, Leonid Dubrovinskaia, Natalia Miyajima, Nobuyoshi Mera, Gabriela Riedel, Ralf Materials (Basel) Article Bulk B-C-N materials were synthesized under static high thermobaric conditions (20 GPa and 2,000 °C) in a multianvil apparatus from a polymer derived t-BC(1.97)N ceramic. The bulk samples were characterised using X-ray synchrotron radiation and analytical transmission electron microscopy in combination with electron energy loss spectroscopy. Polycrystalline B-C-N materials with a cubic type structure were formed under the applied reaction conditions, but the formation of a ternary cubic diamond-like c-BC(2)N compound, could not be unambiguously confirmed. MDPI 2011-11-29 /pmc/articles/PMC5448883/ /pubmed/28824124 http://dx.doi.org/10.3390/ma4122061 Text en © 2011 by the authors. licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Matizamhuka, Wallace R.
Sigalas, Iakovos
Herrmann, Mathias
Dubronvinsky, Leonid
Dubrovinskaia, Natalia
Miyajima, Nobuyoshi
Mera, Gabriela
Riedel, Ralf
Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic
title Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic
title_full Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic
title_fullStr Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic
title_full_unstemmed Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic
title_short Characterization of the Materials Synthesized by High Pressure-High Temperature Treatment of a Polymer Derived t-BC(2)N Ceramic
title_sort characterization of the materials synthesized by high pressure-high temperature treatment of a polymer derived t-bc(2)n ceramic
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5448883/
https://www.ncbi.nlm.nih.gov/pubmed/28824124
http://dx.doi.org/10.3390/ma4122061
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