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Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization
The present paper aims to study the preparation of polyaniline nanofibers through simple interfacial polymerization. Ammonium persulfate, hydrochloric acid and chloroform were used as oxidant, dopant and organic solvent respectively. Field Emission Scanning Electron Microscopy (FESEM), X-ray diffrac...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2012
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5448940/ http://dx.doi.org/10.3390/ma5081487 |
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author | Abdolahi, Ahmad Hamzah, Esah Ibrahim, Zaharah Hashim, Shahrir |
author_facet | Abdolahi, Ahmad Hamzah, Esah Ibrahim, Zaharah Hashim, Shahrir |
author_sort | Abdolahi, Ahmad |
collection | PubMed |
description | The present paper aims to study the preparation of polyaniline nanofibers through simple interfacial polymerization. Ammonium persulfate, hydrochloric acid and chloroform were used as oxidant, dopant and organic solvent respectively. Field Emission Scanning Electron Microscopy (FESEM), X-ray diffraction and Fourier Transform Infrared Spectroscopy (FTIR) techniques were used to analyze the product. FESEM results show that polyaniline has nano-fiber morphology. XRD results show the crystalline properties of polyaniline nanofiber, and FTIR results confirmed the formation of polyaniline in different monomer/oxidant molar ratios. This study provides a better understanding on the synthesis of uniform polyaniline nanofibers through interfacial polymerization. |
format | Online Article Text |
id | pubmed-5448940 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-54489402017-07-28 Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization Abdolahi, Ahmad Hamzah, Esah Ibrahim, Zaharah Hashim, Shahrir Materials (Basel) Article The present paper aims to study the preparation of polyaniline nanofibers through simple interfacial polymerization. Ammonium persulfate, hydrochloric acid and chloroform were used as oxidant, dopant and organic solvent respectively. Field Emission Scanning Electron Microscopy (FESEM), X-ray diffraction and Fourier Transform Infrared Spectroscopy (FTIR) techniques were used to analyze the product. FESEM results show that polyaniline has nano-fiber morphology. XRD results show the crystalline properties of polyaniline nanofiber, and FTIR results confirmed the formation of polyaniline in different monomer/oxidant molar ratios. This study provides a better understanding on the synthesis of uniform polyaniline nanofibers through interfacial polymerization. MDPI 2012-08-22 /pmc/articles/PMC5448940/ http://dx.doi.org/10.3390/ma5081487 Text en © 2012 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/). |
spellingShingle | Article Abdolahi, Ahmad Hamzah, Esah Ibrahim, Zaharah Hashim, Shahrir Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization |
title | Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization |
title_full | Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization |
title_fullStr | Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization |
title_full_unstemmed | Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization |
title_short | Synthesis of Uniform Polyaniline Nanofibers through Interfacial Polymerization |
title_sort | synthesis of uniform polyaniline nanofibers through interfacial polymerization |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5448940/ http://dx.doi.org/10.3390/ma5081487 |
work_keys_str_mv | AT abdolahiahmad synthesisofuniformpolyanilinenanofibersthroughinterfacialpolymerization AT hamzahesah synthesisofuniformpolyanilinenanofibersthroughinterfacialpolymerization AT ibrahimzaharah synthesisofuniformpolyanilinenanofibersthroughinterfacialpolymerization AT hashimshahrir synthesisofuniformpolyanilinenanofibersthroughinterfacialpolymerization |