Cargando…

Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method

In this study, magnesium composites with nano-size boron nitride (BN) particulates of varying contents were synthesized using the powder metallurgy (PM) technique incorporating microwave-assisted two-directional sintering followed by hot extrusion. The effect of nano-BN addition on the microstructur...

Descripción completa

Detalles Bibliográficos
Autores principales: Seetharaman, Sankaranarayanan, Subramanian, Jayalakshmi, Tun, Khin Sandar, Hamouda, Abdelmagid S., Gupta, Manoj
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5452497/
https://www.ncbi.nlm.nih.gov/pubmed/28809252
http://dx.doi.org/10.3390/ma6051940
_version_ 1783240440817909760
author Seetharaman, Sankaranarayanan
Subramanian, Jayalakshmi
Tun, Khin Sandar
Hamouda, Abdelmagid S.
Gupta, Manoj
author_facet Seetharaman, Sankaranarayanan
Subramanian, Jayalakshmi
Tun, Khin Sandar
Hamouda, Abdelmagid S.
Gupta, Manoj
author_sort Seetharaman, Sankaranarayanan
collection PubMed
description In this study, magnesium composites with nano-size boron nitride (BN) particulates of varying contents were synthesized using the powder metallurgy (PM) technique incorporating microwave-assisted two-directional sintering followed by hot extrusion. The effect of nano-BN addition on the microstructural and the mechanical behavior of the developed Mg/BN composites were studied in comparison with pure Mg using the structure-property correlation. Microstructural characterization revealed uniform distribution of nano-BN particulates and marginal grain refinement. The coefficient of thermal expansion (CTE) value of the magnesium matrix was improved with the addition of nano-sized BN particulates. The results of XRD studies indicate basal texture weakening with an increase in nano-BN addition. The composites showed improved mechanical properties measured under micro-indentation, tension and compression loading. While the tensile yield strength improvement was marginal, a significant increase in compressive yield strength was observed. This resulted in the reduction of tension-compression yield asymmetry and can be attributed to the weakening of the strong basal texture.
format Online
Article
Text
id pubmed-5452497
institution National Center for Biotechnology Information
language English
publishDate 2013
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-54524972017-07-28 Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method Seetharaman, Sankaranarayanan Subramanian, Jayalakshmi Tun, Khin Sandar Hamouda, Abdelmagid S. Gupta, Manoj Materials (Basel) Article In this study, magnesium composites with nano-size boron nitride (BN) particulates of varying contents were synthesized using the powder metallurgy (PM) technique incorporating microwave-assisted two-directional sintering followed by hot extrusion. The effect of nano-BN addition on the microstructural and the mechanical behavior of the developed Mg/BN composites were studied in comparison with pure Mg using the structure-property correlation. Microstructural characterization revealed uniform distribution of nano-BN particulates and marginal grain refinement. The coefficient of thermal expansion (CTE) value of the magnesium matrix was improved with the addition of nano-sized BN particulates. The results of XRD studies indicate basal texture weakening with an increase in nano-BN addition. The composites showed improved mechanical properties measured under micro-indentation, tension and compression loading. While the tensile yield strength improvement was marginal, a significant increase in compressive yield strength was observed. This resulted in the reduction of tension-compression yield asymmetry and can be attributed to the weakening of the strong basal texture. MDPI 2013-05-10 /pmc/articles/PMC5452497/ /pubmed/28809252 http://dx.doi.org/10.3390/ma6051940 Text en © 2013 by the authors. licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Seetharaman, Sankaranarayanan
Subramanian, Jayalakshmi
Tun, Khin Sandar
Hamouda, Abdelmagid S.
Gupta, Manoj
Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method
title Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method
title_full Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method
title_fullStr Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method
title_full_unstemmed Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method
title_short Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method
title_sort synthesis and characterization of nano boron nitride reinforced magnesium composites produced by the microwave sintering method
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5452497/
https://www.ncbi.nlm.nih.gov/pubmed/28809252
http://dx.doi.org/10.3390/ma6051940
work_keys_str_mv AT seetharamansankaranarayanan synthesisandcharacterizationofnanoboronnitridereinforcedmagnesiumcompositesproducedbythemicrowavesinteringmethod
AT subramanianjayalakshmi synthesisandcharacterizationofnanoboronnitridereinforcedmagnesiumcompositesproducedbythemicrowavesinteringmethod
AT tunkhinsandar synthesisandcharacterizationofnanoboronnitridereinforcedmagnesiumcompositesproducedbythemicrowavesinteringmethod
AT hamoudaabdelmagids synthesisandcharacterizationofnanoboronnitridereinforcedmagnesiumcompositesproducedbythemicrowavesinteringmethod
AT guptamanoj synthesisandcharacterizationofnanoboronnitridereinforcedmagnesiumcompositesproducedbythemicrowavesinteringmethod