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Simple Preparation of Novel Metal-Containing Mesoporous Starches †

Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m(2) g(−1), being essentially mesoporous with pore sizes in the 10–15 nm ran...

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Detalles Bibliográficos
Autores principales: Ojeda, Manuel, Budarin, Vitaliy, Shuttleworth, Peter S., Clark, James H., Pineda, Antonio, Balu, Alina M., Romero, Antonio A., Luque, Rafael
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5452507/
https://www.ncbi.nlm.nih.gov/pubmed/28809249
http://dx.doi.org/10.3390/ma6051891
Descripción
Sumario:Metal-containing mesoporous starches have been synthesized using a simple and efficient microwave-assisted methodology followed by metal impregnation in the porous gel network. Final materials exhibited surface areas >60 m(2) g(−1), being essentially mesoporous with pore sizes in the 10–15 nm range with some developed inter-particular mesoporosity. These materials characterized by several techniques including XRD, SEM, TG/DTA and DRIFTs may find promising catalytic applications due to the presence of (hydr)oxides in their composition.