Cargando…
A new example of intramolecular C—H⋯Ni anagostic interactions: synthesis, crystal structure and Hirshfeld analysis of cis-bis[4-methyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamidato-κ(2) N (1),S]nickel(II) dimethylformamide monosolvate
The reaction of Ni(II) acetate tetrahydrate with 4-methyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide in a 2:1 molar ratio and recrystallization from dimethylformamide yielded the title compound, [Ni(C(12)H(14)N(3)S)(2)]·C(3)H(7)NO. The ligands act as monoanionic κ(2) N...
Autores principales: | de Oliveira, Adriano Bof, Beck, Johannes, Mellone, Sônia Elizabeth Brown S., Daniels, Jörg |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2017
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5458310/ https://www.ncbi.nlm.nih.gov/pubmed/28638645 http://dx.doi.org/10.1107/S2056989017007198 |
Ejemplares similares
-
Crystal structure of cis-bis[4-phenyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamidato-κ(2)
N
(1),S]nickel(II) monohydrate tetrahydrofuran disolvate
por: de Oliveira, Adriano Bof, et al.
Publicado: (2014) -
Crystal structure of bis[N-phenyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamidato-κ(2)
N
(2),S]zinc dimethyl sulfoxide monosolvate
por: Cruz Santana, Genelane, et al.
Publicado: (2015) -
N-Methyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2014) -
N-Phenyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2014) -
Crystal structure of N-ethyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2017)