Cargando…

Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach

In this report, a technique for rapid synthesis of ZnO microstructures by microwave-assisted heating of precursors at hydrothermal conditions is demonstrated. Further, the reaction mechanism for the growth of ZnO microstructures is analyzed. An accelerated rate of reaction obtained using microwaves...

Descripción completa

Detalles Bibliográficos
Autores principales: Majithia, Ravish, Speich, Jeffrey, Meissner, Kenith E.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5458951/
https://www.ncbi.nlm.nih.gov/pubmed/28809286
http://dx.doi.org/10.3390/ma6062497
_version_ 1783241863827816448
author Majithia, Ravish
Speich, Jeffrey
Meissner, Kenith E.
author_facet Majithia, Ravish
Speich, Jeffrey
Meissner, Kenith E.
author_sort Majithia, Ravish
collection PubMed
description In this report, a technique for rapid synthesis of ZnO microstructures by microwave-assisted heating of precursors at hydrothermal conditions is demonstrated. Further, the reaction mechanism for the growth of ZnO microstructures is analyzed. An accelerated rate of reaction obtained using microwaves enables a dissolution-recrystallization mechanism for generation of one dimensional (1D) rod-like structures, thereby showing that time of reaction can be used to dictate ZnO microstructure morphology.
format Online
Article
Text
id pubmed-5458951
institution National Center for Biotechnology Information
language English
publishDate 2013
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-54589512017-07-28 Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach Majithia, Ravish Speich, Jeffrey Meissner, Kenith E. Materials (Basel) Article In this report, a technique for rapid synthesis of ZnO microstructures by microwave-assisted heating of precursors at hydrothermal conditions is demonstrated. Further, the reaction mechanism for the growth of ZnO microstructures is analyzed. An accelerated rate of reaction obtained using microwaves enables a dissolution-recrystallization mechanism for generation of one dimensional (1D) rod-like structures, thereby showing that time of reaction can be used to dictate ZnO microstructure morphology. MDPI 2013-06-18 /pmc/articles/PMC5458951/ /pubmed/28809286 http://dx.doi.org/10.3390/ma6062497 Text en © 2013 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Majithia, Ravish
Speich, Jeffrey
Meissner, Kenith E.
Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach
title Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach
title_full Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach
title_fullStr Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach
title_full_unstemmed Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach
title_short Mechanism of Generation of ZnO Microstructures by Microwave-Assisted Hydrothermal Approach
title_sort mechanism of generation of zno microstructures by microwave-assisted hydrothermal approach
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5458951/
https://www.ncbi.nlm.nih.gov/pubmed/28809286
http://dx.doi.org/10.3390/ma6062497
work_keys_str_mv AT majithiaravish mechanismofgenerationofznomicrostructuresbymicrowaveassistedhydrothermalapproach
AT speichjeffrey mechanismofgenerationofznomicrostructuresbymicrowaveassistedhydrothermalapproach
AT meissnerkenithe mechanismofgenerationofznomicrostructuresbymicrowaveassistedhydrothermalapproach