Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy

We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid‐state NMR spectroscopy, a thousand‐fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for (13)C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predict...

Descripción completa

Detalles Bibliográficos
Autores principales: Pintér, György, Schwalbe, Harald
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2017
Materias:
Highlights
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5499668/
https://www.ncbi.nlm.nih.gov/pubmed/28544115
http://dx.doi.org/10.1002/anie.201702766
Descripción
Sumario:We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid‐state NMR spectroscopy, a thousand‐fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for (13)C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predicted limitations of high‐field liquid‐state in situ DNP.[Image: see text]

Ejemplares similares