Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy

We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid‐state NMR spectroscopy, a thousand‐fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for (13)C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predict...

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Detalles Bibliográficos
Autores principales: Pintér, György, Schwalbe, Harald
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2017
Materias:
Highlights
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5499668/
https://www.ncbi.nlm.nih.gov/pubmed/28544115
http://dx.doi.org/10.1002/anie.201702766
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author Pintér, György
Schwalbe, Harald
author_facet Pintér, György
Schwalbe, Harald
author_sort Pintér, György
collection PubMed
description We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid‐state NMR spectroscopy, a thousand‐fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for (13)C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predicted limitations of high‐field liquid‐state in situ DNP.[Image: see text]
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spelling pubmed-54996682017-07-21 Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy Pintér, György Schwalbe, Harald Angew Chem Int Ed Engl Highlights We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid‐state NMR spectroscopy, a thousand‐fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for (13)C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predicted limitations of high‐field liquid‐state in situ DNP.[Image: see text] John Wiley and Sons Inc. 2017-05-23 2017-07-10 /pmc/articles/PMC5499668/ /pubmed/28544115 http://dx.doi.org/10.1002/anie.201702766 Text en © 2017 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution‐NonCommercial (http://creativecommons.org/licenses/by-nc/4.0/) License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes.
spellingShingle Highlights
Pintér, György
Schwalbe, Harald
Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy
title Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy
title_full Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy
title_fullStr Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy
title_full_unstemmed Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy
title_short Unprecedented Carbon Signal Enhancement in Liquid‐State NMR Spectroscopy
title_sort unprecedented carbon signal enhancement in liquid‐state nmr spectroscopy
topic Highlights
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5499668/
https://www.ncbi.nlm.nih.gov/pubmed/28544115
http://dx.doi.org/10.1002/anie.201702766
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AT schwalbeharald unprecedentedcarbonsignalenhancementinliquidstatenmrspectroscopy

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