Cargando…
Stability of Nanocrystalline Spark Plasma Sintered 3Y-TZP
Spark plasma sintered 3Y-TZP has been investigated with respect to hydrothermal ageing and grinding. The sintering was performed between the temperatures of 1,100 and 1,600 °C for a soaking time of 5 minutes and the resulting materials were obtained with grain sizes between 65 to 800 nm and relative...
Autores principales: | , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Molecular Diversity Preservation International
2010
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5513509/ http://dx.doi.org/10.3390/ma3020800 |
Sumario: | Spark plasma sintered 3Y-TZP has been investigated with respect to hydrothermal ageing and grinding. The sintering was performed between the temperatures of 1,100 and 1,600 °C for a soaking time of 5 minutes and the resulting materials were obtained with grain sizes between 65 to 800 nm and relative densities between 88.5 to 98.8%. Experiments on hydrothermal ageing in water vapour at 131 °C, 2 bars during 60 hours shows that phase stability is retained, elastic modulus and hardness of near surface region measured by nanoindentation does not change in fine grain (<200 nm) materials, in spite of porosity. In ground specimens, very small amount of transformation was found for all grain sizes studied. |
---|