Cargando…

Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions

This study was focused on the synthesis of silver nanoparticles using Acalypha hispida leaf extract and the characterization of the particles using UV–Vis spectroscopy, XRD, FT-IR, and TEM. The results showed the formation of silver nanoparticles, crystalline in nature, with an average size of 20–50...

Descripción completa

Detalles Bibliográficos
Autores principales: Sithara, R., Selvakumar, P., Arun, C., Anandan, S., Sivashanmugam, P.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5526512/
https://www.ncbi.nlm.nih.gov/pubmed/28765792
http://dx.doi.org/10.1016/j.jare.2017.07.001
_version_ 1783252817333452800
author Sithara, R.
Selvakumar, P.
Arun, C.
Anandan, S.
Sivashanmugam, P.
author_facet Sithara, R.
Selvakumar, P.
Arun, C.
Anandan, S.
Sivashanmugam, P.
author_sort Sithara, R.
collection PubMed
description This study was focused on the synthesis of silver nanoparticles using Acalypha hispida leaf extract and the characterization of the particles using UV–Vis spectroscopy, XRD, FT-IR, and TEM. The results showed the formation of silver nanoparticles, crystalline in nature, with an average size of 20–50 nm. The leaf extract components were analyzed with GC–MS and exhibited a high content of Phytol (40.52%), n-Hexadecanoic acid (9.67%), 1,2,3-Benzenetriol (7.04%), α-d-Mannofuranoside methyl (6.22%), and d-Allose (4.45%). The optimization and statistical investigation of reaction parameters were studied and maximum yield with suitable properties of silver nanoparticles was obtained at leaf extract volume (0.5 mL), the concentration of silver nitrate (1.75 mM), and reaction temperature (50 °C). The method of detecting Mn(2+) ions using the colloidal silver nanoparticles was discussed. The minimum and maximum detection limit were found to be 50 and 200 µM of Mn(II) ions, respectively. Thus, the obtained results encourage the use of economical synthesis of silver nanoparticles in the development of nanosensors to detect the pollutants present in industrial effluents.
format Online
Article
Text
id pubmed-5526512
institution National Center for Biotechnology Information
language English
publishDate 2017
publisher Elsevier
record_format MEDLINE/PubMed
spelling pubmed-55265122017-08-01 Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions Sithara, R. Selvakumar, P. Arun, C. Anandan, S. Sivashanmugam, P. J Adv Res Original Article This study was focused on the synthesis of silver nanoparticles using Acalypha hispida leaf extract and the characterization of the particles using UV–Vis spectroscopy, XRD, FT-IR, and TEM. The results showed the formation of silver nanoparticles, crystalline in nature, with an average size of 20–50 nm. The leaf extract components were analyzed with GC–MS and exhibited a high content of Phytol (40.52%), n-Hexadecanoic acid (9.67%), 1,2,3-Benzenetriol (7.04%), α-d-Mannofuranoside methyl (6.22%), and d-Allose (4.45%). The optimization and statistical investigation of reaction parameters were studied and maximum yield with suitable properties of silver nanoparticles was obtained at leaf extract volume (0.5 mL), the concentration of silver nitrate (1.75 mM), and reaction temperature (50 °C). The method of detecting Mn(2+) ions using the colloidal silver nanoparticles was discussed. The minimum and maximum detection limit were found to be 50 and 200 µM of Mn(II) ions, respectively. Thus, the obtained results encourage the use of economical synthesis of silver nanoparticles in the development of nanosensors to detect the pollutants present in industrial effluents. Elsevier 2017-11 2017-07-10 /pmc/articles/PMC5526512/ /pubmed/28765792 http://dx.doi.org/10.1016/j.jare.2017.07.001 Text en © 2017 Production and hosting by Elsevier B.V. on behalf of Cairo University. https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Original Article
Sithara, R.
Selvakumar, P.
Arun, C.
Anandan, S.
Sivashanmugam, P.
Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions
title Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions
title_full Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions
title_fullStr Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions
title_full_unstemmed Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions
title_short Economical synthesis of silver nanoparticles using leaf extract of Acalypha hispida and its application in the detection of Mn(II) ions
title_sort economical synthesis of silver nanoparticles using leaf extract of acalypha hispida and its application in the detection of mn(ii) ions
topic Original Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5526512/
https://www.ncbi.nlm.nih.gov/pubmed/28765792
http://dx.doi.org/10.1016/j.jare.2017.07.001
work_keys_str_mv AT sitharar economicalsynthesisofsilvernanoparticlesusingleafextractofacalyphahispidaanditsapplicationinthedetectionofmniiions
AT selvakumarp economicalsynthesisofsilvernanoparticlesusingleafextractofacalyphahispidaanditsapplicationinthedetectionofmniiions
AT arunc economicalsynthesisofsilvernanoparticlesusingleafextractofacalyphahispidaanditsapplicationinthedetectionofmniiions
AT anandans economicalsynthesisofsilvernanoparticlesusingleafextractofacalyphahispidaanditsapplicationinthedetectionofmniiions
AT sivashanmugamp economicalsynthesisofsilvernanoparticlesusingleafextractofacalyphahispidaanditsapplicationinthedetectionofmniiions