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Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses
Iron oxide ornamented carbon nanotube nanocomposites (Fe(3)O(4).CNT NCs) were prepared by a wet-chemical process in basic means. The optical, morphological, and structural characterizations of Fe(3)O(4).CNT NCs were performed using FTIR, UV/Vis., FESEM, TEM; XEDS, XPS, and XRD respectively. Flat GCE...
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Public Library of Science
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5609863/ https://www.ncbi.nlm.nih.gov/pubmed/28938019 http://dx.doi.org/10.1371/journal.pone.0177817 |
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author | Rahman, Mohammed M. Hussain, Mohammad Musarraf Asiri, Abdullah M. |
author_facet | Rahman, Mohammed M. Hussain, Mohammad Musarraf Asiri, Abdullah M. |
author_sort | Rahman, Mohammed M. |
collection | PubMed |
description | Iron oxide ornamented carbon nanotube nanocomposites (Fe(3)O(4).CNT NCs) were prepared by a wet-chemical process in basic means. The optical, morphological, and structural characterizations of Fe(3)O(4).CNT NCs were performed using FTIR, UV/Vis., FESEM, TEM; XEDS, XPS, and XRD respectively. Flat GCE had been fabricated with a thin-layer of NCs using a coating binding agent. It was performed for the chemical sensor development by a dependable I-V technique. Among all interfering analytes, 3-methoxyphenol (3-MP) was selective towards the fabricated sensor. Increased electrochemical performances for example elevated sensitivity, linear dynamic range (LDR) and continuing steadiness towards selective 3-MP had been observed with chemical sensor. The calibration graph found linear (R(2) = 0.9340) in a wide range of 3-MP concentration (90.0 pM ~ 90.0 mM). The limit of detection and sensitivity were considered as 1.0 pM and 9×10(−4) μAμM(-1)cm(-2) respectively. The prepared of Fe(3)O(4).CNT NCs by a wet-chemical progression is an interesting route for the development of hazardous phenolic sensor based on nanocomposite materials. It is also recommended that 3-MP sensor is exhibited a promising performances based on Fe(3)O(4).CNT NCs by a facile I-V method for the significant applications of toxic chemicals for the safety of environmental and health-care fields. |
format | Online Article Text |
id | pubmed-5609863 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2017 |
publisher | Public Library of Science |
record_format | MEDLINE/PubMed |
spelling | pubmed-56098632017-10-17 Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses Rahman, Mohammed M. Hussain, Mohammad Musarraf Asiri, Abdullah M. PLoS One Research Article Iron oxide ornamented carbon nanotube nanocomposites (Fe(3)O(4).CNT NCs) were prepared by a wet-chemical process in basic means. The optical, morphological, and structural characterizations of Fe(3)O(4).CNT NCs were performed using FTIR, UV/Vis., FESEM, TEM; XEDS, XPS, and XRD respectively. Flat GCE had been fabricated with a thin-layer of NCs using a coating binding agent. It was performed for the chemical sensor development by a dependable I-V technique. Among all interfering analytes, 3-methoxyphenol (3-MP) was selective towards the fabricated sensor. Increased electrochemical performances for example elevated sensitivity, linear dynamic range (LDR) and continuing steadiness towards selective 3-MP had been observed with chemical sensor. The calibration graph found linear (R(2) = 0.9340) in a wide range of 3-MP concentration (90.0 pM ~ 90.0 mM). The limit of detection and sensitivity were considered as 1.0 pM and 9×10(−4) μAμM(-1)cm(-2) respectively. The prepared of Fe(3)O(4).CNT NCs by a wet-chemical progression is an interesting route for the development of hazardous phenolic sensor based on nanocomposite materials. It is also recommended that 3-MP sensor is exhibited a promising performances based on Fe(3)O(4).CNT NCs by a facile I-V method for the significant applications of toxic chemicals for the safety of environmental and health-care fields. Public Library of Science 2017-09-22 /pmc/articles/PMC5609863/ /pubmed/28938019 http://dx.doi.org/10.1371/journal.pone.0177817 Text en © 2017 Rahman et al http://creativecommons.org/licenses/by/4.0/ This is an open access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/) , which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. |
spellingShingle | Research Article Rahman, Mohammed M. Hussain, Mohammad Musarraf Asiri, Abdullah M. Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses |
title | Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses |
title_full | Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses |
title_fullStr | Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses |
title_full_unstemmed | Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses |
title_short | Fabrication of 3-methoxyphenol sensor based on Fe(3)O(4) decorated carbon nanotube nanocomposites for environmental safety: Real sample analyses |
title_sort | fabrication of 3-methoxyphenol sensor based on fe(3)o(4) decorated carbon nanotube nanocomposites for environmental safety: real sample analyses |
topic | Research Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5609863/ https://www.ncbi.nlm.nih.gov/pubmed/28938019 http://dx.doi.org/10.1371/journal.pone.0177817 |
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