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Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites

A polymer nanocomposite was produced by ultrasonic-assisted dispersion of multiwalled carbon nanotubes (MWCNTs) in a polycarbonate matrix using p-xylene and dichloromethane as the solvents. The filler loading was varied from 1 to 3 wt % in order to examine the effect of MWCNTs on the structure and p...

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Autores principales: Larosa, Claudio, Patra, Niranjan, Salerno, Marco, Mikac, Lara, Merijs Meri, Remo, Ivanda, Mile
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5629402/
https://www.ncbi.nlm.nih.gov/pubmed/29046850
http://dx.doi.org/10.3762/bjnano.8.203
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author Larosa, Claudio
Patra, Niranjan
Salerno, Marco
Mikac, Lara
Merijs Meri, Remo
Ivanda, Mile
author_facet Larosa, Claudio
Patra, Niranjan
Salerno, Marco
Mikac, Lara
Merijs Meri, Remo
Ivanda, Mile
author_sort Larosa, Claudio
collection PubMed
description A polymer nanocomposite was produced by ultrasonic-assisted dispersion of multiwalled carbon nanotubes (MWCNTs) in a polycarbonate matrix using p-xylene and dichloromethane as the solvents. The filler loading was varied from 1 to 3 wt % in order to examine the effect of MWCNTs on the structure and properties of the composites. The nanocomposites were characterized by DSC, DTA, TGA, UV–vis, FTIR and Raman spectroscopy to evaluate the changes induced by the filler in the polymer matrix. UV–vis, FTIR and Raman spectroscopy measurements confirmed the presence of the dispersed phase in the composite films, while TGA and DSC analysis of the nanocomposites revealed enhanced thermal stability and decreased crystallinity, respectively, as compared to the neat polymer. The proposed composites can find application in a number of everyday products where polycarbonate is the base polymer.
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spelling pubmed-56294022017-10-18 Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites Larosa, Claudio Patra, Niranjan Salerno, Marco Mikac, Lara Merijs Meri, Remo Ivanda, Mile Beilstein J Nanotechnol Full Research Paper A polymer nanocomposite was produced by ultrasonic-assisted dispersion of multiwalled carbon nanotubes (MWCNTs) in a polycarbonate matrix using p-xylene and dichloromethane as the solvents. The filler loading was varied from 1 to 3 wt % in order to examine the effect of MWCNTs on the structure and properties of the composites. The nanocomposites were characterized by DSC, DTA, TGA, UV–vis, FTIR and Raman spectroscopy to evaluate the changes induced by the filler in the polymer matrix. UV–vis, FTIR and Raman spectroscopy measurements confirmed the presence of the dispersed phase in the composite films, while TGA and DSC analysis of the nanocomposites revealed enhanced thermal stability and decreased crystallinity, respectively, as compared to the neat polymer. The proposed composites can find application in a number of everyday products where polycarbonate is the base polymer. Beilstein-Institut 2017-09-27 /pmc/articles/PMC5629402/ /pubmed/29046850 http://dx.doi.org/10.3762/bjnano.8.203 Text en Copyright © 2017, Larosa et al. https://creativecommons.org/licenses/by/4.0https://www.beilstein-journals.org/bjnano/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Nanotechnology terms and conditions: (https://www.beilstein-journals.org/bjnano/terms)
spellingShingle Full Research Paper
Larosa, Claudio
Patra, Niranjan
Salerno, Marco
Mikac, Lara
Merijs Meri, Remo
Ivanda, Mile
Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
title Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
title_full Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
title_fullStr Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
title_full_unstemmed Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
title_short Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
title_sort preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5629402/
https://www.ncbi.nlm.nih.gov/pubmed/29046850
http://dx.doi.org/10.3762/bjnano.8.203
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