Synthesis of 4H‐Benzo[e][1,3]oxazin‐4‐ones by a Carbonylation–Cyclization Domino Reaction of ortho‐Halophenols and Cyanamide

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A mild and convenient one‐step preparation of 4H‐1,3‐benzoxazin‐4‐ones by a domino carbonylation–cyclization process is developed. Readily available ortho‐iodophenols are subjected to palladium‐catalyzed carbonylative coupling with Mo(CO)(6) and cyanamide, followed by a spontaneous, intramolecular c...

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Detalles Bibliográficos
Autores principales: Åkerbladh, Linda, Chow, Shiao Y., Odell, Luke R., Larhed, Mats
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2017
Materias:
Full Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5641915/
https://www.ncbi.nlm.nih.gov/pubmed/29046856
http://dx.doi.org/10.1002/open.201700130

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5641915/
https://www.ncbi.nlm.nih.gov/pubmed/29046856
http://dx.doi.org/10.1002/open.201700130

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