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Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process

INTRODUCTION: Essential oil is consisting of complex component. It is divided into major and minor component. Therefore, this study aims to examine the distribution of major and minor components on Kaffir lime oil by using fractional distillation. Fractional distillation and distributional analysis...

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Autores principales: Warsito, Warsito, Palungan, Maimunah Hindun, Utomo, Edy Priyo
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The African Field Epidemiology Network 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5660901/
https://www.ncbi.nlm.nih.gov/pubmed/29187951
http://dx.doi.org/10.11604/pamj.2017.27.282.9679
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author Warsito, Warsito
Palungan, Maimunah Hindun
Utomo, Edy Priyo
author_facet Warsito, Warsito
Palungan, Maimunah Hindun
Utomo, Edy Priyo
author_sort Warsito, Warsito
collection PubMed
description INTRODUCTION: Essential oil is consisting of complex component. It is divided into major and minor component. Therefore, this study aims to examine the distribution of major and minor components on Kaffir lime oil by using fractional distillation. Fractional distillation and distributional analysis of components within fractions have been performed on kaffir lime oil (Citrus hystrix DC.). METHODS: Fractional distillation was performed by using PiloDist 104-VTU, column length of 2 m (number of plate 120), the system pressure was set on 5 and 10 mBar, while the reflux ratio varied on 10/10, 20/10 and 60/10, and the chemical composition analysis was done by using GC-MS. Chemical composition of the distillated lime oil consisted of mix-twigs and leaves that composed of 20 compounds, with five main components β-citronellal (46.40%), L-linalool (13.11%), β-citronellol (11.03%), citronelyl acetate (6.76%) and sabinen (5.91%). RESULTS: The optimum conditions for fractional distillation were obtained at 5 mBar pressure with reflux ratio of 10/10. Components of β -citronellal and L-linalool were distributed in the fraction-1 to fraction 9, hydrocarbon monoterpenes components were distributed only on the fraction-1 to fraction 4, while the oxygenated monoterpenes components dominated the fraction-5 to fraction-9. CONCLUSION: The highest level of β-citronellal was 84.86% (fraction-7), L-linalool 20.13% (fraction-5), sabinen 19.83% (fraction-1), and the component level of 4-terpeneol, β-citronellol and sitronelyl acetate respectively 7.16%; 12.27%; 5.22% (fraction-9).
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spelling pubmed-56609012017-11-29 Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process Warsito, Warsito Palungan, Maimunah Hindun Utomo, Edy Priyo Pan Afr Med J Research INTRODUCTION: Essential oil is consisting of complex component. It is divided into major and minor component. Therefore, this study aims to examine the distribution of major and minor components on Kaffir lime oil by using fractional distillation. Fractional distillation and distributional analysis of components within fractions have been performed on kaffir lime oil (Citrus hystrix DC.). METHODS: Fractional distillation was performed by using PiloDist 104-VTU, column length of 2 m (number of plate 120), the system pressure was set on 5 and 10 mBar, while the reflux ratio varied on 10/10, 20/10 and 60/10, and the chemical composition analysis was done by using GC-MS. Chemical composition of the distillated lime oil consisted of mix-twigs and leaves that composed of 20 compounds, with five main components β-citronellal (46.40%), L-linalool (13.11%), β-citronellol (11.03%), citronelyl acetate (6.76%) and sabinen (5.91%). RESULTS: The optimum conditions for fractional distillation were obtained at 5 mBar pressure with reflux ratio of 10/10. Components of β -citronellal and L-linalool were distributed in the fraction-1 to fraction 9, hydrocarbon monoterpenes components were distributed only on the fraction-1 to fraction 4, while the oxygenated monoterpenes components dominated the fraction-5 to fraction-9. CONCLUSION: The highest level of β-citronellal was 84.86% (fraction-7), L-linalool 20.13% (fraction-5), sabinen 19.83% (fraction-1), and the component level of 4-terpeneol, β-citronellol and sitronelyl acetate respectively 7.16%; 12.27%; 5.22% (fraction-9). The African Field Epidemiology Network 2017-08-21 /pmc/articles/PMC5660901/ /pubmed/29187951 http://dx.doi.org/10.11604/pamj.2017.27.282.9679 Text en © Warsito Warsito et al. http://creativecommons.org/licenses/by/2.0/ The Pan African Medical Journal - ISSN 1937-8688. This is an Open Access article distributed under the terms of the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Research
Warsito, Warsito
Palungan, Maimunah Hindun
Utomo, Edy Priyo
Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process
title Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process
title_full Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process
title_fullStr Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process
title_full_unstemmed Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process
title_short Profiling study of the major and minor components of kaffir lime oil (Citrus hystrix DC.) in the fractional distillation process
title_sort profiling study of the major and minor components of kaffir lime oil (citrus hystrix dc.) in the fractional distillation process
topic Research
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5660901/
https://www.ncbi.nlm.nih.gov/pubmed/29187951
http://dx.doi.org/10.11604/pamj.2017.27.282.9679
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