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Unusual thermolysis of azacyclic allene under microwave conditions: crystal structure of (3RS,3aSR,8RS,8aRS)-methyl 5,6-dimethoxy-3a,10-dimethyl-1-phenyl-3,3a,8,8a-tetrahydro-3,8-(epiminomethano)cyclopenta[a]indene-2-carboxylate from synchrotron X-ray diffraction
The title compound, C(25)H(27)NO(4) (I), the product of the unusual thermolysis of azacyclic allene methyl 10,11-dimethoxy-3,8-dimethyl-6-phenyl-3-azabenzo[d]cyclodeca-4,6,7-triene-5-carboxylate, represents a bicyclic heterosystem and crystallizes in the monoclinic space group P2(1)/c with thre...
Autores principales: | Anh, Le Tuan, Titov, Alexander A., Kobzev, Maxim S., Voskressensky, Leonid G., Varlamov, Alexey V., Dorovatovskii, Pavel V., Khrustalev, Victor N. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5683510/ https://www.ncbi.nlm.nih.gov/pubmed/29152370 http://dx.doi.org/10.1107/S2056989017014864 |
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