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Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate)
In the title compound, C(29)H(25)FN(2)O(4), the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115 Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0 (5)°; the benzene ring is twisted with respect to the mean planes of the two indole...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5683515/ https://www.ncbi.nlm.nih.gov/pubmed/29152375 http://dx.doi.org/10.1107/S2056989017015523 |
Sumario: | In the title compound, C(29)H(25)FN(2)O(4), the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115 Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0 (5)°; the benzene ring is twisted with respect to the mean planes of the two indole ring systems by 83.3 (2) and 88.1 (4)°, respectively. In the crystal, pairs of N—H⋯O hydrogen bonds link the molecules into centrosymmetric dimers, which are further linked by N—H⋯O hydrogen bonds into supramolecular chains propagating along the [101] direction. |
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