Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate

In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluene­sulfonamide ring and the combined ring system involving the pyridone and benzo­thia­zole rings subtend an inter­planar angle of 39.86 (4)°. The pyridone and benzo­thiazyl rings are linked by the intra­molecular hydrogen bond N—H(a...

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Autores principales: Azzam, Rasha A., Elgemeie, Galal H., Elsayed, Rasha E., Jones, Peter G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2017
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5730231/
https://www.ncbi.nlm.nih.gov/pubmed/29250394
http://dx.doi.org/10.1107/S2056989017015778
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author Azzam, Rasha A.
Elgemeie, Galal H.
Elsayed, Rasha E.
Jones, Peter G.
author_facet Azzam, Rasha A.
Elgemeie, Galal H.
Elsayed, Rasha E.
Jones, Peter G.
author_sort Azzam, Rasha A.
collection PubMed
description In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluene­sulfonamide ring and the combined ring system involving the pyridone and benzo­thia­zole rings subtend an inter­planar angle of 39.86 (4)°. The pyridone and benzo­thiazyl rings are linked by the intra­molecular hydrogen bond N—H(amine)⋯N(thia­zole). The DMF O atom accepts two classical hydrogen bonds. The mol­ecules are linked by hydrogen bonds and an S⋯O contact to form layers parallel to the bc plane.
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spelling pubmed-57302312017-12-15 Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate Azzam, Rasha A. Elgemeie, Galal H. Elsayed, Rasha E. Jones, Peter G. Acta Crystallogr E Crystallogr Commun Research Communications In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluene­sulfonamide ring and the combined ring system involving the pyridone and benzo­thia­zole rings subtend an inter­planar angle of 39.86 (4)°. The pyridone and benzo­thiazyl rings are linked by the intra­molecular hydrogen bond N—H(amine)⋯N(thia­zole). The DMF O atom accepts two classical hydrogen bonds. The mol­ecules are linked by hydrogen bonds and an S⋯O contact to form layers parallel to the bc plane. International Union of Crystallography 2017-11-03 /pmc/articles/PMC5730231/ /pubmed/29250394 http://dx.doi.org/10.1107/S2056989017015778 Text en © Azzam et al. 2017 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/
spellingShingle Research Communications
Azzam, Rasha A.
Elgemeie, Galal H.
Elsayed, Rasha E.
Jones, Peter G.
Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
title Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
title_full Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
title_fullStr Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
title_full_unstemmed Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
title_short Crystal structure of N-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
title_sort crystal structure of n-[6-amino-5-(benzo[d]thia­zol-2-yl)-3-cyano-4-methyl­sulfanyl-2-oxo-1,2-di­hydro­pyridin-1-yl]-4-methyl­benzene­sulfonamide di­methyl­formamide monosolvate
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5730231/
https://www.ncbi.nlm.nih.gov/pubmed/29250394
http://dx.doi.org/10.1107/S2056989017015778
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