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Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate
In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluenesulfonamide ring and the combined ring system involving the pyridone and benzothiazole rings subtend an interplanar angle of 39.86 (4)°. The pyridone and benzothiazyl rings are linked by the intramolecular hydrogen bond N—H(a...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5730231/ https://www.ncbi.nlm.nih.gov/pubmed/29250394 http://dx.doi.org/10.1107/S2056989017015778 |
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author | Azzam, Rasha A. Elgemeie, Galal H. Elsayed, Rasha E. Jones, Peter G. |
author_facet | Azzam, Rasha A. Elgemeie, Galal H. Elsayed, Rasha E. Jones, Peter G. |
author_sort | Azzam, Rasha A. |
collection | PubMed |
description | In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluenesulfonamide ring and the combined ring system involving the pyridone and benzothiazole rings subtend an interplanar angle of 39.86 (4)°. The pyridone and benzothiazyl rings are linked by the intramolecular hydrogen bond N—H(amine)⋯N(thiazole). The DMF O atom accepts two classical hydrogen bonds. The molecules are linked by hydrogen bonds and an S⋯O contact to form layers parallel to the bc plane. |
format | Online Article Text |
id | pubmed-5730231 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2017 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-57302312017-12-15 Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate Azzam, Rasha A. Elgemeie, Galal H. Elsayed, Rasha E. Jones, Peter G. Acta Crystallogr E Crystallogr Commun Research Communications In the title compound, C(21)H(17)N(5)O(3)S(3)·C(3)H(7)NO, the toluenesulfonamide ring and the combined ring system involving the pyridone and benzothiazole rings subtend an interplanar angle of 39.86 (4)°. The pyridone and benzothiazyl rings are linked by the intramolecular hydrogen bond N—H(amine)⋯N(thiazole). The DMF O atom accepts two classical hydrogen bonds. The molecules are linked by hydrogen bonds and an S⋯O contact to form layers parallel to the bc plane. International Union of Crystallography 2017-11-03 /pmc/articles/PMC5730231/ /pubmed/29250394 http://dx.doi.org/10.1107/S2056989017015778 Text en © Azzam et al. 2017 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/ |
spellingShingle | Research Communications Azzam, Rasha A. Elgemeie, Galal H. Elsayed, Rasha E. Jones, Peter G. Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
title | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
title_full | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
title_fullStr | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
title_full_unstemmed | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
title_short | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
title_sort | crystal structure of n-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
topic | Research Communications |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5730231/ https://www.ncbi.nlm.nih.gov/pubmed/29250394 http://dx.doi.org/10.1107/S2056989017015778 |
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