Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection

A new method for the determination of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection (MCE-CCD) was proposed. The effects of various electrophoretic operating parameters on the analysis of arecoline were studied. Under the opt...

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Detalles Bibliográficos
Autores principales: Cai, Zi-You, Li, Yong-Chong, Li, Li-Hua, Chen, Zuan-Guang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Xi'an Jiaotong University 2012
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5760757/
https://www.ncbi.nlm.nih.gov/pubmed/29403766
http://dx.doi.org/10.1016/j.jpha.2012.07.003
Descripción
Sumario:A new method for the determination of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection (MCE-CCD) was proposed. The effects of various electrophoretic operating parameters on the analysis of arecoline were studied. Under the optimal conditions, arecoline was rapidly separated and detected in 1 min with good linearity over the concentration range of 20–1500 μM (r(2)=0.9991) and the detection limit of 5 μM (S/N=3). The method was used for the analysis of arecoline satisfactorily with a recovery of 96.8–104%.

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