Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection

A new method for the determination of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection (MCE-CCD) was proposed. The effects of various electrophoretic operating parameters on the analysis of arecoline were studied. Under the opt...

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Detalles Bibliográficos
Autores principales: Cai, Zi-You, Li, Yong-Chong, Li, Li-Hua, Chen, Zuan-Guang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Xi'an Jiaotong University 2012
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5760757/
https://www.ncbi.nlm.nih.gov/pubmed/29403766
http://dx.doi.org/10.1016/j.jpha.2012.07.003
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author Cai, Zi-You
Li, Yong-Chong
Li, Li-Hua
Chen, Zuan-Guang
author_facet Cai, Zi-You
Li, Yong-Chong
Li, Li-Hua
Chen, Zuan-Guang
author_sort Cai, Zi-You
collection PubMed
description A new method for the determination of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection (MCE-CCD) was proposed. The effects of various electrophoretic operating parameters on the analysis of arecoline were studied. Under the optimal conditions, arecoline was rapidly separated and detected in 1 min with good linearity over the concentration range of 20–1500 μM (r(2)=0.9991) and the detection limit of 5 μM (S/N=3). The method was used for the analysis of arecoline satisfactorily with a recovery of 96.8–104%.
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spelling pubmed-57607572018-02-05 Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection Cai, Zi-You Li, Yong-Chong Li, Li-Hua Chen, Zuan-Guang J Pharm Anal Article A new method for the determination of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection (MCE-CCD) was proposed. The effects of various electrophoretic operating parameters on the analysis of arecoline were studied. Under the optimal conditions, arecoline was rapidly separated and detected in 1 min with good linearity over the concentration range of 20–1500 μM (r(2)=0.9991) and the detection limit of 5 μM (S/N=3). The method was used for the analysis of arecoline satisfactorily with a recovery of 96.8–104%. Xi'an Jiaotong University 2012-10 2012-07-11 /pmc/articles/PMC5760757/ /pubmed/29403766 http://dx.doi.org/10.1016/j.jpha.2012.07.003 Text en © 2012 Xi'an Jiaotong University http://creativecommons.org/licenses/by-nc-nd/3.0/ This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/3.0/).
spellingShingle Article
Cai, Zi-You
Li, Yong-Chong
Li, Li-Hua
Chen, Zuan-Guang
Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
title Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
title_full Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
title_fullStr Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
title_full_unstemmed Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
title_short Analysis of arecoline in Semen Arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
title_sort analysis of arecoline in semen arecae decoction pieces by microchip capillary electrophoresis with contactless conductivity detection
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5760757/
https://www.ncbi.nlm.nih.gov/pubmed/29403766
http://dx.doi.org/10.1016/j.jpha.2012.07.003
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