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Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry

Volatile components from Rhizoma Alpiniae Officinarum were respectively extracted by three methods including hydrodistillation, headspace solid-phase microextraction (HS-SPME) and diethyl ether extraction. A total of 40 (hydrodistillation), 32 (HS-SPME) and 37 (diethyl ether extraction) compounds we...

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Autores principales: Xie, Zhi-Sheng, Xu, Xin-Jun, Xie, Chun-Yan, Huang, Jie-Yun, Yang, Mei, Yang, De-Po
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Xi'an Jiaotong University 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5760953/
https://www.ncbi.nlm.nih.gov/pubmed/29403820
http://dx.doi.org/10.1016/j.jpha.2012.09.005
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author Xie, Zhi-Sheng
Xu, Xin-Jun
Xie, Chun-Yan
Huang, Jie-Yun
Yang, Mei
Yang, De-Po
author_facet Xie, Zhi-Sheng
Xu, Xin-Jun
Xie, Chun-Yan
Huang, Jie-Yun
Yang, Mei
Yang, De-Po
author_sort Xie, Zhi-Sheng
collection PubMed
description Volatile components from Rhizoma Alpiniae Officinarum were respectively extracted by three methods including hydrodistillation, headspace solid-phase microextraction (HS-SPME) and diethyl ether extraction. A total of 40 (hydrodistillation), 32 (HS-SPME) and 37 (diethyl ether extraction) compounds were respectively identified by gas chromatography–mass spectrometry (GC/MS) and 22 compounds were overlapped, including α-farnesene, γ-muurolene, 2,6-dimethyl-6-(4-methyl-3-pentenyl)bicyclo[3.1.1]hept-2-ene, eucalyptol and cadina-1(10), 4-diene and so forth, varying in relative contents. HS-SPME is fast, sample saving and solvent-free and it also can achieve similar profiles as those from hydrodistillation and solvent extraction. Therefore, it can be the priority for extracting volatile components from medicinal plants.
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spelling pubmed-57609532018-02-05 Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry Xie, Zhi-Sheng Xu, Xin-Jun Xie, Chun-Yan Huang, Jie-Yun Yang, Mei Yang, De-Po J Pharm Anal Article Volatile components from Rhizoma Alpiniae Officinarum were respectively extracted by three methods including hydrodistillation, headspace solid-phase microextraction (HS-SPME) and diethyl ether extraction. A total of 40 (hydrodistillation), 32 (HS-SPME) and 37 (diethyl ether extraction) compounds were respectively identified by gas chromatography–mass spectrometry (GC/MS) and 22 compounds were overlapped, including α-farnesene, γ-muurolene, 2,6-dimethyl-6-(4-methyl-3-pentenyl)bicyclo[3.1.1]hept-2-ene, eucalyptol and cadina-1(10), 4-diene and so forth, varying in relative contents. HS-SPME is fast, sample saving and solvent-free and it also can achieve similar profiles as those from hydrodistillation and solvent extraction. Therefore, it can be the priority for extracting volatile components from medicinal plants. Xi'an Jiaotong University 2013-06 2012-10-07 /pmc/articles/PMC5760953/ /pubmed/29403820 http://dx.doi.org/10.1016/j.jpha.2012.09.005 Text en © 2013 Xian Jiaotong University. Production and hosting by Elsevier B.V. http://creativecommons.org/licenses/by-nc-nd/3.0/ This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/3.0/).
spellingShingle Article
Xie, Zhi-Sheng
Xu, Xin-Jun
Xie, Chun-Yan
Huang, Jie-Yun
Yang, Mei
Yang, De-Po
Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
title Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
title_full Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
title_fullStr Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
title_full_unstemmed Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
title_short Volatile components of Rhizoma Alpiniae Officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
title_sort volatile components of rhizoma alpiniae officinarum using three different extraction methods combined with gas chromatography–mass spectrometry
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5760953/
https://www.ncbi.nlm.nih.gov/pubmed/29403820
http://dx.doi.org/10.1016/j.jpha.2012.09.005
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