Preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus by high-speed counter-current chromatography

A high-speed counter-current chromatography (HSCCC) method was successfully developed for the preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus in one step. The purity of deoxyschizandrin was 98.5%, and the structure was identified by MS, UV and NMR....

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Detalles Bibliográficos
Autores principales: Li, Xin-Ying, Yang, Mei, Huang, Jie-Yun, Yu, Xiao-Xue, Zhao, Min-Qian, Liang, Zhi-Kun, Xie, Zhi-Sheng, Xu, Xin-Jun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Xi'an Jiaotong University 2013
Materias:
Original Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5761001/
https://www.ncbi.nlm.nih.gov/pubmed/29403850
http://dx.doi.org/10.1016/j.jpha.2013.07.002
Descripción
Sumario:A high-speed counter-current chromatography (HSCCC) method was successfully developed for the preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus in one step. The purity of deoxyschizandrin was 98.5%, and the structure was identified by MS, UV and NMR. This method was simple, fast, convenient and appropriate to prepare pure compound as reference substances for related research on Schisandrae Sphenantherae Fructus.

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