A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide

N,N′-Methylenebisacrylamide (MBAA), which is an important raw material in a widely industrial area, was synthesized using convenient catalysts. The synthesized monomer was fully characterized by the elemental analysis, fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA)...

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Autores principales: Avşar, Abdullah, Gökbulut, Yener, Ay, Burak, Serin, Selahattin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Taylor & Francis 2017
Materias:
Articles
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5798195/
https://www.ncbi.nlm.nih.gov/pubmed/29491814
http://dx.doi.org/10.1080/15685551.2017.1332138
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author Avşar, Abdullah
Gökbulut, Yener
Ay, Burak
Serin, Selahattin
author_facet Avşar, Abdullah
Gökbulut, Yener
Ay, Burak
Serin, Selahattin
author_sort Avşar, Abdullah
collection PubMed
description N,N′-Methylenebisacrylamide (MBAA), which is an important raw material in a widely industrial area, was synthesized using convenient catalysts. The synthesized monomer was fully characterized by the elemental analysis, fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA), (1)H-NMR, (13)C-NMR, GC/MS, and high performance liquid chromatography (HPLC) analysis. Six different homogeneous and heterogeneous catalysts were used to obtain maximum monomer yield. The MBAA was obtained with 95% yield by using Cu(II) catalyst containing carboxylate groups ligands.
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spelling pubmed-57981952018-02-28 A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide Avşar, Abdullah Gökbulut, Yener Ay, Burak Serin, Selahattin Des Monomers Polym Articles N,N′-Methylenebisacrylamide (MBAA), which is an important raw material in a widely industrial area, was synthesized using convenient catalysts. The synthesized monomer was fully characterized by the elemental analysis, fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA), (1)H-NMR, (13)C-NMR, GC/MS, and high performance liquid chromatography (HPLC) analysis. Six different homogeneous and heterogeneous catalysts were used to obtain maximum monomer yield. The MBAA was obtained with 95% yield by using Cu(II) catalyst containing carboxylate groups ligands. Taylor & Francis 2017-05-26 /pmc/articles/PMC5798195/ /pubmed/29491814 http://dx.doi.org/10.1080/15685551.2017.1332138 Text en © 2017 The Author(s). Published by Informa UK Limited, trading as Taylor & Francis Group http://creativecommons.org/licenses/by/4.0/ This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Articles
Avşar, Abdullah
Gökbulut, Yener
Ay, Burak
Serin, Selahattin
A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
title A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
title_full A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
title_fullStr A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
title_full_unstemmed A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
title_short A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
title_sort novel catalyst system for the synthesis of n,n′-methylenebisacrylamide from acrylamide
topic Articles
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5798195/
https://www.ncbi.nlm.nih.gov/pubmed/29491814
http://dx.doi.org/10.1080/15685551.2017.1332138
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