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Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology

Stable isotope analysis has been utilized in archaeology since the 1970s, yet standardized protocols for terminology, sampling, pretreatment evaluation, calibration, quality assurance and control, data presentation, and graphical or statistical treatment still remain lacking in archaeological applic...

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Autores principales: Roberts, Patrick, Fernandes, Ricardo, Craig, Oliver E., Larsen, Thomas, Lucquin, Alexandre, Swift, Jillian, Zech, Jana
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5838555/
https://www.ncbi.nlm.nih.gov/pubmed/29235694
http://dx.doi.org/10.1002/rcm.8044
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author Roberts, Patrick
Fernandes, Ricardo
Craig, Oliver E.
Larsen, Thomas
Lucquin, Alexandre
Swift, Jillian
Zech, Jana
author_facet Roberts, Patrick
Fernandes, Ricardo
Craig, Oliver E.
Larsen, Thomas
Lucquin, Alexandre
Swift, Jillian
Zech, Jana
author_sort Roberts, Patrick
collection PubMed
description Stable isotope analysis has been utilized in archaeology since the 1970s, yet standardized protocols for terminology, sampling, pretreatment evaluation, calibration, quality assurance and control, data presentation, and graphical or statistical treatment still remain lacking in archaeological applications. Here, we present recommendations and requirements for each of these in the archaeological context of: bulk stable carbon and nitrogen isotope analysis of organics; bulk stable carbon and oxygen isotope analysis of carbonates; single compound stable carbon and nitrogen isotope analysis on amino acids in collagen and keratin; and single compound stable carbon and hydrogen isotope analysis on fatty acids. The protocols are based on recommendations from the Commission on Isotopic Abundances and Atomic Weights of the International Union of Pure and Applied Chemistry (IUPAC) as well as an expanding geochemical and archaeological science experimental literature. We hope that this will provide a useful future reference for authors and reviewers engaging with the growing number of stable isotope applications and datasets in archaeology.
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spelling pubmed-58385552018-03-12 Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology Roberts, Patrick Fernandes, Ricardo Craig, Oliver E. Larsen, Thomas Lucquin, Alexandre Swift, Jillian Zech, Jana Rapid Commun Mass Spectrom Protocols Stable isotope analysis has been utilized in archaeology since the 1970s, yet standardized protocols for terminology, sampling, pretreatment evaluation, calibration, quality assurance and control, data presentation, and graphical or statistical treatment still remain lacking in archaeological applications. Here, we present recommendations and requirements for each of these in the archaeological context of: bulk stable carbon and nitrogen isotope analysis of organics; bulk stable carbon and oxygen isotope analysis of carbonates; single compound stable carbon and nitrogen isotope analysis on amino acids in collagen and keratin; and single compound stable carbon and hydrogen isotope analysis on fatty acids. The protocols are based on recommendations from the Commission on Isotopic Abundances and Atomic Weights of the International Union of Pure and Applied Chemistry (IUPAC) as well as an expanding geochemical and archaeological science experimental literature. We hope that this will provide a useful future reference for authors and reviewers engaging with the growing number of stable isotope applications and datasets in archaeology. John Wiley and Sons Inc. 2018-02-08 2018-03-15 /pmc/articles/PMC5838555/ /pubmed/29235694 http://dx.doi.org/10.1002/rcm.8044 Text en © 2017 The Authors. Rapid Communications in Mass Spectrometry Pubished by John Wiley & Sons Ltd. This is an open access article under the terms of the Creative Commons Attribution (http://creativecommons.org/licenses/by/4.0/) License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.
spellingShingle Protocols
Roberts, Patrick
Fernandes, Ricardo
Craig, Oliver E.
Larsen, Thomas
Lucquin, Alexandre
Swift, Jillian
Zech, Jana
Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
title Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
title_full Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
title_fullStr Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
title_full_unstemmed Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
title_short Calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
title_sort calling all archaeologists: guidelines for terminology, methodology, data handling, and reporting when undertaking and reviewing stable isotope applications in archaeology
topic Protocols
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5838555/
https://www.ncbi.nlm.nih.gov/pubmed/29235694
http://dx.doi.org/10.1002/rcm.8044
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