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Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites

Out-of-autoclave prepreg typically needs a long cure cycle to guarantee good properties as the result of low processing pressure applied. It is essential to reduce the manufacturing time, achieve real cost reduction, and take full advantage of out-of-autoclave process. The focus of this paper is to...

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Detalles Bibliográficos
Autores principales: Dong, Anqi, Zhao, Yan, Zhao, Xinqing, Yu, Qiyong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5873000/
https://www.ncbi.nlm.nih.gov/pubmed/29534048
http://dx.doi.org/10.3390/ma11030421
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author Dong, Anqi
Zhao, Yan
Zhao, Xinqing
Yu, Qiyong
author_facet Dong, Anqi
Zhao, Yan
Zhao, Xinqing
Yu, Qiyong
author_sort Dong, Anqi
collection PubMed
description Out-of-autoclave prepreg typically needs a long cure cycle to guarantee good properties as the result of low processing pressure applied. It is essential to reduce the manufacturing time, achieve real cost reduction, and take full advantage of out-of-autoclave process. The focus of this paper is to reduce the cure cycle time and production cost while maintaining high laminate quality. A rapidly cured out-of-autoclave resin and relative prepreg were independently developed. To determine a suitable rapid cure procedure for the developed prepreg, the effect of heating rate, initial cure temperature, dwelling time, and post-cure time on the final laminate quality were evaluated and the factors were then optimized. As a result, a rapid cure procedure was determined. The results showed that the resin infiltration could be completed at the end of the initial cure stage and no obvious void could be seen in the laminate at this time. The laminate could achieve good internal quality using the optimized cure procedure. The mechanical test results showed that the laminates had a fiber volume fraction of 59–60% with a final glass transition temperature of 205 °C and excellent mechanical strength especially the flexural properties.
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spelling pubmed-58730002018-03-30 Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites Dong, Anqi Zhao, Yan Zhao, Xinqing Yu, Qiyong Materials (Basel) Article Out-of-autoclave prepreg typically needs a long cure cycle to guarantee good properties as the result of low processing pressure applied. It is essential to reduce the manufacturing time, achieve real cost reduction, and take full advantage of out-of-autoclave process. The focus of this paper is to reduce the cure cycle time and production cost while maintaining high laminate quality. A rapidly cured out-of-autoclave resin and relative prepreg were independently developed. To determine a suitable rapid cure procedure for the developed prepreg, the effect of heating rate, initial cure temperature, dwelling time, and post-cure time on the final laminate quality were evaluated and the factors were then optimized. As a result, a rapid cure procedure was determined. The results showed that the resin infiltration could be completed at the end of the initial cure stage and no obvious void could be seen in the laminate at this time. The laminate could achieve good internal quality using the optimized cure procedure. The mechanical test results showed that the laminates had a fiber volume fraction of 59–60% with a final glass transition temperature of 205 °C and excellent mechanical strength especially the flexural properties. MDPI 2018-03-13 /pmc/articles/PMC5873000/ /pubmed/29534048 http://dx.doi.org/10.3390/ma11030421 Text en © 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Dong, Anqi
Zhao, Yan
Zhao, Xinqing
Yu, Qiyong
Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites
title Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites
title_full Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites
title_fullStr Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites
title_full_unstemmed Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites
title_short Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites
title_sort cure cycle optimization of rapidly cured out-of-autoclave composites
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5873000/
https://www.ncbi.nlm.nih.gov/pubmed/29534048
http://dx.doi.org/10.3390/ma11030421
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