Cargando…
Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces
Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept p...
Autores principales: | , , , , , , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2018
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5929362/ https://www.ncbi.nlm.nih.gov/pubmed/29714205 http://dx.doi.org/10.1107/S1600577518004848 |
_version_ | 1783319391240192000 |
---|---|
author | Larsen, Simon R. Hansteen, Marie Pacakova, Barbara Theodor, Keld Arnold, Thomas Rennie, Adrian R. Helgesen, Geir Knudsen, Kenneth D. Bordallo, Heloisa N. Fossum, Jon Otto Cavalcanti, Leide P. |
author_facet | Larsen, Simon R. Hansteen, Marie Pacakova, Barbara Theodor, Keld Arnold, Thomas Rennie, Adrian R. Helgesen, Geir Knudsen, Kenneth D. Bordallo, Heloisa N. Fossum, Jon Otto Cavalcanti, Leide P. |
author_sort | Larsen, Simon R. |
collection | PubMed |
description | Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source. |
format | Online Article Text |
id | pubmed-5929362 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2018 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-59293622018-05-11 Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces Larsen, Simon R. Hansteen, Marie Pacakova, Barbara Theodor, Keld Arnold, Thomas Rennie, Adrian R. Helgesen, Geir Knudsen, Kenneth D. Bordallo, Heloisa N. Fossum, Jon Otto Cavalcanti, Leide P. J Synchrotron Radiat Laboratory Notes Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air–liquid and liquid–liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source. International Union of Crystallography 2018-04-24 /pmc/articles/PMC5929362/ /pubmed/29714205 http://dx.doi.org/10.1107/S1600577518004848 Text en © Simon R. Larse et al. 2018 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/ |
spellingShingle | Laboratory Notes Larsen, Simon R. Hansteen, Marie Pacakova, Barbara Theodor, Keld Arnold, Thomas Rennie, Adrian R. Helgesen, Geir Knudsen, Kenneth D. Bordallo, Heloisa N. Fossum, Jon Otto Cavalcanti, Leide P. Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces |
title | Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces |
title_full | Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces |
title_fullStr | Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces |
title_full_unstemmed | Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces |
title_short | Sample cell for studying liquid interfaces with an in situ electric field using X-ray reflectivity and application to clay particles at oil–oil interfaces |
title_sort | sample cell for studying liquid interfaces with an in situ electric field using x-ray reflectivity and application to clay particles at oil–oil interfaces |
topic | Laboratory Notes |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5929362/ https://www.ncbi.nlm.nih.gov/pubmed/29714205 http://dx.doi.org/10.1107/S1600577518004848 |
work_keys_str_mv | AT larsensimonr samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT hansteenmarie samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT pacakovabarbara samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT theodorkeld samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT arnoldthomas samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT rennieadrianr samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT helgesengeir samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT knudsenkennethd samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT bordalloheloisan samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT fossumjonotto samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces AT cavalcantileidep samplecellforstudyingliquidinterfaceswithaninsituelectricfieldusingxrayreflectivityandapplicationtoclayparticlesatoiloilinterfaces |