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Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
BACKGROUND: The purpose of this in vitro study was to evaluate the effect of conventional surface treatment with acid solutions on the surface roughness of a zirconia-based ceramic. MATERIAL AND METHODS: Specimens of yttrium-tetragonal zirconia polycrystal (Y-TZP) -based ceramic were fabricated (5.0...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Medicina Oral S.L.
2018
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5937956/ https://www.ncbi.nlm.nih.gov/pubmed/29750098 http://dx.doi.org/10.4317/jced.54571 |
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author | Goyatá, Frederico Galvão, Yvna Simões, Thamyryz-Rafaela Goyatá, Luiz-Felipe Arruda, José-Alcides Moreno, Amália |
author_facet | Goyatá, Frederico Galvão, Yvna Simões, Thamyryz-Rafaela Goyatá, Luiz-Felipe Arruda, José-Alcides Moreno, Amália |
author_sort | Goyatá, Frederico |
collection | PubMed |
description | BACKGROUND: The purpose of this in vitro study was to evaluate the effect of conventional surface treatment with acid solutions on the surface roughness of a zirconia-based ceramic. MATERIAL AND METHODS: Specimens of yttrium-tetragonal zirconia polycrystal (Y-TZP) -based ceramic were fabricated (5.0 x 5.0 x 2.0 mm, n=40). The specimens were submitted to the tested surface treatment method and divided into 4 groups (n=10): no treatment-control (GI), airborne 110 µm aluminum oxide particle abrasion for 1 minute-conventional method (GII); etching with 48% hydrofluoric acid for 2 minutes (GIII), and nitric acid/hydrofluoric acid etching for 2 minutes (GIV). The surface roughness (Ra) test was performed, followed by AFM analysis. The results were analyzed by ANOVA and the Tukey test, with the level of significance set at a=.05. RESULTS: The surface treatment with acid solutions (0.16 ± 0.02-GIII; 0.11 ± 0.01-GIV) promoted a significant increase in roughness, with higher mean Ra values of Y-TZP (μm) compared to control (0.06 ± 0.01-GI) (p >.05), and lower values compared to the conventional method (0.21 ± 0.06-GII). The aluminum oxide particle treatment resulted in deep microretentions forming sharp Y-TZP peaks compared to only microretentions with acid solution treatments. CONCLUSIONS: All Y-TZP treatments effectively promoted microretention in the ceramic. Hydrofluoric acid (48%) proved to be more effective in increasing the Ra of Y-TZP than the nitric acid/hydrofluoric acid treatment. Atomic force microscopy images revealed that both acid solutions modified the surface of the Y-TZP in a uniform manner. Key words:Zirconia, surface modification, roughness, yttria-stabilized tetragonal zirconia polycrystal. |
format | Online Article Text |
id | pubmed-5937956 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2018 |
publisher | Medicina Oral S.L. |
record_format | MEDLINE/PubMed |
spelling | pubmed-59379562018-05-10 Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal Goyatá, Frederico Galvão, Yvna Simões, Thamyryz-Rafaela Goyatá, Luiz-Felipe Arruda, José-Alcides Moreno, Amália J Clin Exp Dent Research BACKGROUND: The purpose of this in vitro study was to evaluate the effect of conventional surface treatment with acid solutions on the surface roughness of a zirconia-based ceramic. MATERIAL AND METHODS: Specimens of yttrium-tetragonal zirconia polycrystal (Y-TZP) -based ceramic were fabricated (5.0 x 5.0 x 2.0 mm, n=40). The specimens were submitted to the tested surface treatment method and divided into 4 groups (n=10): no treatment-control (GI), airborne 110 µm aluminum oxide particle abrasion for 1 minute-conventional method (GII); etching with 48% hydrofluoric acid for 2 minutes (GIII), and nitric acid/hydrofluoric acid etching for 2 minutes (GIV). The surface roughness (Ra) test was performed, followed by AFM analysis. The results were analyzed by ANOVA and the Tukey test, with the level of significance set at a=.05. RESULTS: The surface treatment with acid solutions (0.16 ± 0.02-GIII; 0.11 ± 0.01-GIV) promoted a significant increase in roughness, with higher mean Ra values of Y-TZP (μm) compared to control (0.06 ± 0.01-GI) (p >.05), and lower values compared to the conventional method (0.21 ± 0.06-GII). The aluminum oxide particle treatment resulted in deep microretentions forming sharp Y-TZP peaks compared to only microretentions with acid solution treatments. CONCLUSIONS: All Y-TZP treatments effectively promoted microretention in the ceramic. Hydrofluoric acid (48%) proved to be more effective in increasing the Ra of Y-TZP than the nitric acid/hydrofluoric acid treatment. Atomic force microscopy images revealed that both acid solutions modified the surface of the Y-TZP in a uniform manner. Key words:Zirconia, surface modification, roughness, yttria-stabilized tetragonal zirconia polycrystal. Medicina Oral S.L. 2018-04-01 /pmc/articles/PMC5937956/ /pubmed/29750098 http://dx.doi.org/10.4317/jced.54571 Text en Copyright: © 2018 Medicina Oral S.L. http://creativecommons.org/licenses/by/2.5/ This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. |
spellingShingle | Research Goyatá, Frederico Galvão, Yvna Simões, Thamyryz-Rafaela Goyatá, Luiz-Felipe Arruda, José-Alcides Moreno, Amália Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal |
title | Effect of surface treatments with acid solutions on the surface
roughness of an Yttrium-Tetragonal Zirconia Polycrystal |
title_full | Effect of surface treatments with acid solutions on the surface
roughness of an Yttrium-Tetragonal Zirconia Polycrystal |
title_fullStr | Effect of surface treatments with acid solutions on the surface
roughness of an Yttrium-Tetragonal Zirconia Polycrystal |
title_full_unstemmed | Effect of surface treatments with acid solutions on the surface
roughness of an Yttrium-Tetragonal Zirconia Polycrystal |
title_short | Effect of surface treatments with acid solutions on the surface
roughness of an Yttrium-Tetragonal Zirconia Polycrystal |
title_sort | effect of surface treatments with acid solutions on the surface
roughness of an yttrium-tetragonal zirconia polycrystal |
topic | Research |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5937956/ https://www.ncbi.nlm.nih.gov/pubmed/29750098 http://dx.doi.org/10.4317/jced.54571 |
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