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Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal

BACKGROUND: The purpose of this in vitro study was to evaluate the effect of conventional surface treatment with acid solutions on the surface roughness of a zirconia-based ceramic. MATERIAL AND METHODS: Specimens of yttrium-tetragonal zirconia polycrystal (Y-TZP) -based ceramic were fabricated (5.0...

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Autores principales: Goyatá, Frederico, Galvão, Yvna, Simões, Thamyryz-Rafaela, Goyatá, Luiz-Felipe, Arruda, José-Alcides, Moreno, Amália
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Medicina Oral S.L. 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5937956/
https://www.ncbi.nlm.nih.gov/pubmed/29750098
http://dx.doi.org/10.4317/jced.54571
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author Goyatá, Frederico
Galvão, Yvna
Simões, Thamyryz-Rafaela
Goyatá, Luiz-Felipe
Arruda, José-Alcides
Moreno, Amália
author_facet Goyatá, Frederico
Galvão, Yvna
Simões, Thamyryz-Rafaela
Goyatá, Luiz-Felipe
Arruda, José-Alcides
Moreno, Amália
author_sort Goyatá, Frederico
collection PubMed
description BACKGROUND: The purpose of this in vitro study was to evaluate the effect of conventional surface treatment with acid solutions on the surface roughness of a zirconia-based ceramic. MATERIAL AND METHODS: Specimens of yttrium-tetragonal zirconia polycrystal (Y-TZP) -based ceramic were fabricated (5.0 x 5.0 x 2.0 mm, n=40). The specimens were submitted to the tested surface treatment method and divided into 4 groups (n=10): no treatment-control (GI), airborne 110 µm aluminum oxide particle abrasion for 1 minute-conventional method (GII); etching with 48% hydrofluoric acid for 2 minutes (GIII), and nitric acid/hydrofluoric acid etching for 2 minutes (GIV). The surface roughness (Ra) test was performed, followed by AFM analysis. The results were analyzed by ANOVA and the Tukey test, with the level of significance set at a=.05. RESULTS: The surface treatment with acid solutions (0.16 ± 0.02-GIII; 0.11 ± 0.01-GIV) promoted a significant increase in roughness, with higher mean Ra values of Y-TZP (μm) compared to control (0.06 ± 0.01-GI) (p >.05), and lower values compared to the conventional method (0.21 ± 0.06-GII). The aluminum oxide particle treatment resulted in deep microretentions forming sharp Y-TZP peaks compared to only microretentions with acid solution treatments. CONCLUSIONS: All Y-TZP treatments effectively promoted microretention in the ceramic. Hydrofluoric acid (48%) proved to be more effective in increasing the Ra of Y-TZP than the nitric acid/hydrofluoric acid treatment. Atomic force microscopy images revealed that both acid solutions modified the surface of the Y-TZP in a uniform manner. Key words:Zirconia, surface modification, roughness, yttria-stabilized tetragonal zirconia polycrystal.
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spelling pubmed-59379562018-05-10 Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal Goyatá, Frederico Galvão, Yvna Simões, Thamyryz-Rafaela Goyatá, Luiz-Felipe Arruda, José-Alcides Moreno, Amália J Clin Exp Dent Research BACKGROUND: The purpose of this in vitro study was to evaluate the effect of conventional surface treatment with acid solutions on the surface roughness of a zirconia-based ceramic. MATERIAL AND METHODS: Specimens of yttrium-tetragonal zirconia polycrystal (Y-TZP) -based ceramic were fabricated (5.0 x 5.0 x 2.0 mm, n=40). The specimens were submitted to the tested surface treatment method and divided into 4 groups (n=10): no treatment-control (GI), airborne 110 µm aluminum oxide particle abrasion for 1 minute-conventional method (GII); etching with 48% hydrofluoric acid for 2 minutes (GIII), and nitric acid/hydrofluoric acid etching for 2 minutes (GIV). The surface roughness (Ra) test was performed, followed by AFM analysis. The results were analyzed by ANOVA and the Tukey test, with the level of significance set at a=.05. RESULTS: The surface treatment with acid solutions (0.16 ± 0.02-GIII; 0.11 ± 0.01-GIV) promoted a significant increase in roughness, with higher mean Ra values of Y-TZP (μm) compared to control (0.06 ± 0.01-GI) (p >.05), and lower values compared to the conventional method (0.21 ± 0.06-GII). The aluminum oxide particle treatment resulted in deep microretentions forming sharp Y-TZP peaks compared to only microretentions with acid solution treatments. CONCLUSIONS: All Y-TZP treatments effectively promoted microretention in the ceramic. Hydrofluoric acid (48%) proved to be more effective in increasing the Ra of Y-TZP than the nitric acid/hydrofluoric acid treatment. Atomic force microscopy images revealed that both acid solutions modified the surface of the Y-TZP in a uniform manner. Key words:Zirconia, surface modification, roughness, yttria-stabilized tetragonal zirconia polycrystal. Medicina Oral S.L. 2018-04-01 /pmc/articles/PMC5937956/ /pubmed/29750098 http://dx.doi.org/10.4317/jced.54571 Text en Copyright: © 2018 Medicina Oral S.L. http://creativecommons.org/licenses/by/2.5/ This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Research
Goyatá, Frederico
Galvão, Yvna
Simões, Thamyryz-Rafaela
Goyatá, Luiz-Felipe
Arruda, José-Alcides
Moreno, Amália
Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
title Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
title_full Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
title_fullStr Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
title_full_unstemmed Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
title_short Effect of surface treatments with acid solutions on the surface roughness of an Yttrium-Tetragonal Zirconia Polycrystal
title_sort effect of surface treatments with acid solutions on the surface roughness of an yttrium-tetragonal zirconia polycrystal
topic Research
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5937956/
https://www.ncbi.nlm.nih.gov/pubmed/29750098
http://dx.doi.org/10.4317/jced.54571
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