Electron crystallography with the EIGER detector

Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a...

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Autores principales: Tinti, Gemma, Fröjdh, Erik, van Genderen, Eric, Gruene, Tim, Schmitt, Bernd, de Winter, D. A. Matthijs, Weckhuysen, Bert M., Abrahams, Jan Pieter
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2018
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5947724/
https://www.ncbi.nlm.nih.gov/pubmed/29765609
http://dx.doi.org/10.1107/S2052252518000945
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author Tinti, Gemma
Fröjdh, Erik
van Genderen, Eric
Gruene, Tim
Schmitt, Bernd
de Winter, D. A. Matthijs
Weckhuysen, Bert M.
Abrahams, Jan Pieter
author_facet Tinti, Gemma
Fröjdh, Erik
van Genderen, Eric
Gruene, Tim
Schmitt, Bernd
de Winter, D. A. Matthijs
Weckhuysen, Bert M.
Abrahams, Jan Pieter
author_sort Tinti, Gemma
collection PubMed
description Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a transmission electron microscope. EIGER features a pixel pitch of 75 × 75 µm(2), frame rates up to 23 kHz and a dead time between frames as low as 3 µs. Cluster size and modulation transfer functions of the detector at 100, 200 and 300 keV electron energies are reported and the data quality is demonstrated by structure determination of a SAPO-34 zeotype from electron diffraction data.
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spelling pubmed-59477242018-05-15 Electron crystallography with the EIGER detector Tinti, Gemma Fröjdh, Erik van Genderen, Eric Gruene, Tim Schmitt, Bernd de Winter, D. A. Matthijs Weckhuysen, Bert M. Abrahams, Jan Pieter IUCrJ Research Papers Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a transmission electron microscope. EIGER features a pixel pitch of 75 × 75 µm(2), frame rates up to 23 kHz and a dead time between frames as low as 3 µs. Cluster size and modulation transfer functions of the detector at 100, 200 and 300 keV electron energies are reported and the data quality is demonstrated by structure determination of a SAPO-34 zeotype from electron diffraction data. International Union of Crystallography 2018-02-14 /pmc/articles/PMC5947724/ /pubmed/29765609 http://dx.doi.org/10.1107/S2052252518000945 Text en © Gemma Tinti et al. 2018 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/
spellingShingle Research Papers
Tinti, Gemma
Fröjdh, Erik
van Genderen, Eric
Gruene, Tim
Schmitt, Bernd
de Winter, D. A. Matthijs
Weckhuysen, Bert M.
Abrahams, Jan Pieter
Electron crystallography with the EIGER detector
title Electron crystallography with the EIGER detector
title_full Electron crystallography with the EIGER detector
title_fullStr Electron crystallography with the EIGER detector
title_full_unstemmed Electron crystallography with the EIGER detector
title_short Electron crystallography with the EIGER detector
title_sort electron crystallography with the eiger detector
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5947724/
https://www.ncbi.nlm.nih.gov/pubmed/29765609
http://dx.doi.org/10.1107/S2052252518000945
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