Cargando…

Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres

In this paper, pure and Ag-doped SnO(2) nanospheres were synthesized by hydrothermal method and characterized via X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), and X-ray photoelectron spectra (XPS), respectively. The gas se...

Descripción completa

Detalles Bibliográficos
Autores principales: Lu, Zhaorui, Zhou, Qu, Xu, Lingna, Gui, Yingang, Zhao, Zhongyong, Tang, Chao, Chen, Weigen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5951338/
https://www.ncbi.nlm.nih.gov/pubmed/29587421
http://dx.doi.org/10.3390/ma11040492
_version_ 1783323006216437760
author Lu, Zhaorui
Zhou, Qu
Xu, Lingna
Gui, Yingang
Zhao, Zhongyong
Tang, Chao
Chen, Weigen
author_facet Lu, Zhaorui
Zhou, Qu
Xu, Lingna
Gui, Yingang
Zhao, Zhongyong
Tang, Chao
Chen, Weigen
author_sort Lu, Zhaorui
collection PubMed
description In this paper, pure and Ag-doped SnO(2) nanospheres were synthesized by hydrothermal method and characterized via X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), and X-ray photoelectron spectra (XPS), respectively. The gas sensing performance of the pure, 1 at.%, 3 at.%, and 5 at.% Ag-doped SnO(2) sensing devices toward hydrogen (H(2)) were systematically evaluated. The results indicated that compared with pure SnO(2) nanospheres, Ag-doped SnO(2) nanospheres could not only decrease the optimum working temperature but also significantly improve H(2) sensing such as higher gas response and faster response-recovery. Among all the samples, the 3 at.% Ag-doped SnO(2) showed the highest response 39 to 100 μL/L H(2) at 300 °C. Moreover, its gas sensing mechanism was discussed, and the results will provide reference and theoretical guidance for the development of high-performance SnO(2)-based H(2) sensing devices.
format Online
Article
Text
id pubmed-5951338
institution National Center for Biotechnology Information
language English
publishDate 2018
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-59513382018-05-15 Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres Lu, Zhaorui Zhou, Qu Xu, Lingna Gui, Yingang Zhao, Zhongyong Tang, Chao Chen, Weigen Materials (Basel) Article In this paper, pure and Ag-doped SnO(2) nanospheres were synthesized by hydrothermal method and characterized via X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), and X-ray photoelectron spectra (XPS), respectively. The gas sensing performance of the pure, 1 at.%, 3 at.%, and 5 at.% Ag-doped SnO(2) sensing devices toward hydrogen (H(2)) were systematically evaluated. The results indicated that compared with pure SnO(2) nanospheres, Ag-doped SnO(2) nanospheres could not only decrease the optimum working temperature but also significantly improve H(2) sensing such as higher gas response and faster response-recovery. Among all the samples, the 3 at.% Ag-doped SnO(2) showed the highest response 39 to 100 μL/L H(2) at 300 °C. Moreover, its gas sensing mechanism was discussed, and the results will provide reference and theoretical guidance for the development of high-performance SnO(2)-based H(2) sensing devices. MDPI 2018-03-26 /pmc/articles/PMC5951338/ /pubmed/29587421 http://dx.doi.org/10.3390/ma11040492 Text en © 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Lu, Zhaorui
Zhou, Qu
Xu, Lingna
Gui, Yingang
Zhao, Zhongyong
Tang, Chao
Chen, Weigen
Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres
title Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres
title_full Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres
title_fullStr Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres
title_full_unstemmed Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres
title_short Synthesis and Characterization of Highly Sensitive Hydrogen (H(2)) Sensing Device Based on Ag Doped SnO(2) Nanospheres
title_sort synthesis and characterization of highly sensitive hydrogen (h(2)) sensing device based on ag doped sno(2) nanospheres
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5951338/
https://www.ncbi.nlm.nih.gov/pubmed/29587421
http://dx.doi.org/10.3390/ma11040492
work_keys_str_mv AT luzhaorui synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres
AT zhouqu synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres
AT xulingna synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres
AT guiyingang synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres
AT zhaozhongyong synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres
AT tangchao synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres
AT chenweigen synthesisandcharacterizationofhighlysensitivehydrogenh2sensingdevicebasedonagdopedsno2nanospheres