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Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide

Mol­ecules of the title compound, C(24)H(8)F(4)N(2)O(8), have C (i) point-group symmetry in the crystal, as they lie on crystallographic inversion centres (Z′ = 1/2). The di­fluoro­phenyl ring is disordered over two orientations; the final refined occupancy factors of the two components of disorder...

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Autores principales: Fusco, Sandra, Tuzi, Angela, Centore, Roberto, Carella, Antonio
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5956342/
https://www.ncbi.nlm.nih.gov/pubmed/29850059
http://dx.doi.org/10.1107/S2056989018001226
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author Fusco, Sandra
Tuzi, Angela
Centore, Roberto
Carella, Antonio
author_facet Fusco, Sandra
Tuzi, Angela
Centore, Roberto
Carella, Antonio
author_sort Fusco, Sandra
collection PubMed
description Mol­ecules of the title compound, C(24)H(8)F(4)N(2)O(8), have C (i) point-group symmetry in the crystal, as they lie on crystallographic inversion centres (Z′ = 1/2). The di­fluoro­phenyl ring is disordered over two orientations; the final refined occupancy factors of the two components of disorder are 0.947 (4) and 0.053 (4). In the crystal, some C(ar)—H⋯F inter­actions are present, which involve the most acidic H atom of the mol­ecule.
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spelling pubmed-59563422018-05-30 Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide Fusco, Sandra Tuzi, Angela Centore, Roberto Carella, Antonio Acta Crystallogr E Crystallogr Commun Research Communications Mol­ecules of the title compound, C(24)H(8)F(4)N(2)O(8), have C (i) point-group symmetry in the crystal, as they lie on crystallographic inversion centres (Z′ = 1/2). The di­fluoro­phenyl ring is disordered over two orientations; the final refined occupancy factors of the two components of disorder are 0.947 (4) and 0.053 (4). In the crystal, some C(ar)—H⋯F inter­actions are present, which involve the most acidic H atom of the mol­ecule. International Union of Crystallography 2018-01-26 /pmc/articles/PMC5956342/ /pubmed/29850059 http://dx.doi.org/10.1107/S2056989018001226 Text en © Fusco et al. 2018 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/
spellingShingle Research Communications
Fusco, Sandra
Tuzi, Angela
Centore, Roberto
Carella, Antonio
Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
title Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
title_full Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
title_fullStr Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
title_full_unstemmed Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
title_short Crystal structure of N,N′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
title_sort crystal structure of n,n′-bis­(2,4-di­fluoro­benzo­yloxy)benzene-1,2:4,5-tetra­carboximide
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5956342/
https://www.ncbi.nlm.nih.gov/pubmed/29850059
http://dx.doi.org/10.1107/S2056989018001226
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