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Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide
Molecules of the title compound, C(24)H(8)F(4)N(2)O(8), have C (i) point-group symmetry in the crystal, as they lie on crystallographic inversion centres (Z′ = 1/2). The difluorophenyl ring is disordered over two orientations; the final refined occupancy factors of the two components of disorder...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2018
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5956342/ https://www.ncbi.nlm.nih.gov/pubmed/29850059 http://dx.doi.org/10.1107/S2056989018001226 |
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author | Fusco, Sandra Tuzi, Angela Centore, Roberto Carella, Antonio |
author_facet | Fusco, Sandra Tuzi, Angela Centore, Roberto Carella, Antonio |
author_sort | Fusco, Sandra |
collection | PubMed |
description | Molecules of the title compound, C(24)H(8)F(4)N(2)O(8), have C (i) point-group symmetry in the crystal, as they lie on crystallographic inversion centres (Z′ = 1/2). The difluorophenyl ring is disordered over two orientations; the final refined occupancy factors of the two components of disorder are 0.947 (4) and 0.053 (4). In the crystal, some C(ar)—H⋯F interactions are present, which involve the most acidic H atom of the molecule. |
format | Online Article Text |
id | pubmed-5956342 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2018 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-59563422018-05-30 Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide Fusco, Sandra Tuzi, Angela Centore, Roberto Carella, Antonio Acta Crystallogr E Crystallogr Commun Research Communications Molecules of the title compound, C(24)H(8)F(4)N(2)O(8), have C (i) point-group symmetry in the crystal, as they lie on crystallographic inversion centres (Z′ = 1/2). The difluorophenyl ring is disordered over two orientations; the final refined occupancy factors of the two components of disorder are 0.947 (4) and 0.053 (4). In the crystal, some C(ar)—H⋯F interactions are present, which involve the most acidic H atom of the molecule. International Union of Crystallography 2018-01-26 /pmc/articles/PMC5956342/ /pubmed/29850059 http://dx.doi.org/10.1107/S2056989018001226 Text en © Fusco et al. 2018 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/ |
spellingShingle | Research Communications Fusco, Sandra Tuzi, Angela Centore, Roberto Carella, Antonio Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
title | Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
title_full | Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
title_fullStr | Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
title_full_unstemmed | Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
title_short | Crystal structure of N,N′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
title_sort | crystal structure of n,n′-bis(2,4-difluorobenzoyloxy)benzene-1,2:4,5-tetracarboximide |
topic | Research Communications |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5956342/ https://www.ncbi.nlm.nih.gov/pubmed/29850059 http://dx.doi.org/10.1107/S2056989018001226 |
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