Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate

In the title azo­pyrrole compound, C(17)H(15)N(3)O(2)·CH(3)OH, the azo N=N bond adopts a trans configuration and the pyrrole N and azo group are in an anti orientation. The dihedral angles between the pyrrole ring and the two phenyl rings are 6.7 (3) and 54.7 (3)°. In the crystal, a supra­molecular...

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Detalles Bibliográficos
Autores principales: Yang, Guiwen, Feng, Huixiao, Yin, Zhenming
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2018
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6002831/
https://www.ncbi.nlm.nih.gov/pubmed/29951248
http://dx.doi.org/10.1107/S2056989018007764
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author Yang, Guiwen
Feng, Huixiao
Yin, Zhenming
author_facet Yang, Guiwen
Feng, Huixiao
Yin, Zhenming
author_sort Yang, Guiwen
collection PubMed
description In the title azo­pyrrole compound, C(17)H(15)N(3)O(2)·CH(3)OH, the azo N=N bond adopts a trans configuration and the pyrrole N and azo group are in an anti orientation. The dihedral angles between the pyrrole ring and the two phenyl rings are 6.7 (3) and 54.7 (3)°. In the crystal, a supra­molecular ring structure is formed between two azo­pyrrole and two methanol solvent mol­ecules through four O—H⋯O hydrogen bonds.
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spelling pubmed-60028312018-06-27 Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate Yang, Guiwen Feng, Huixiao Yin, Zhenming Acta Crystallogr E Crystallogr Commun Research Communications In the title azo­pyrrole compound, C(17)H(15)N(3)O(2)·CH(3)OH, the azo N=N bond adopts a trans configuration and the pyrrole N and azo group are in an anti orientation. The dihedral angles between the pyrrole ring and the two phenyl rings are 6.7 (3) and 54.7 (3)°. In the crystal, a supra­molecular ring structure is formed between two azo­pyrrole and two methanol solvent mol­ecules through four O—H⋯O hydrogen bonds. International Union of Crystallography 2018-05-31 /pmc/articles/PMC6002831/ /pubmed/29951248 http://dx.doi.org/10.1107/S2056989018007764 Text en © Yang et al. 2018 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/
spellingShingle Research Communications
Yang, Guiwen
Feng, Huixiao
Yin, Zhenming
Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
title Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
title_full Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
title_fullStr Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
title_full_unstemmed Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
title_short Crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
title_sort crystal structure of 2-{5-[2-(2-hy­droxy­phen­yl)diazen-1-yl]-1-methyl­pyrrol-2-yl}phenol methanol monosolvate
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6002831/
https://www.ncbi.nlm.nih.gov/pubmed/29951248
http://dx.doi.org/10.1107/S2056989018007764
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AT yinzhenming crystalstructureof2522hydroxyphenyldiazen1yl1methylpyrrol2ylphenolmethanolmonosolvate

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