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Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties
Furan resin and fir powder pretreated by FeCl(3) and aqueous ammonia solution were used to fabricate α-Fe/Fe(3)C/woodceramic nanocomposite. The bands of the pretreated wood powder were characterized by Fourier transform infrared spectroscopy (FTIR). The structural characterization of the nanocomposi...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2018
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6024902/ https://www.ncbi.nlm.nih.gov/pubmed/29794971 http://dx.doi.org/10.3390/ma11060878 |
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author | Zhou, Weihong Yu, Yunshui Xiong, Xueliang Zhou, Sicong |
author_facet | Zhou, Weihong Yu, Yunshui Xiong, Xueliang Zhou, Sicong |
author_sort | Zhou, Weihong |
collection | PubMed |
description | Furan resin and fir powder pretreated by FeCl(3) and aqueous ammonia solution were used to fabricate α-Fe/Fe(3)C/woodceramic nanocomposite. The bands of the pretreated wood powder were characterized by Fourier transform infrared spectroscopy (FTIR). The structural characterization of the nanocomposites was performed by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The microwave absorption of the nanocomposites was measured by a vector network analyzer in the range of 2–18 GHz. The mechanical properties of the composites were also investigated. XRD and SEM results show that the α-Fe and Fe(3)C nanoparticles are in-situ generated and disperse in the matrix of the woodceramic. The diameters of these nanoparticles increase with the increasing of concentration of FeCl(3) solution. The experimental results show that both the complex permittivity and the complex permeability of α-Fe/Fe(3)C/woodceramic nanocomposites increase as the concentration of FeCl(3) solution increases. The composites pretreated with 0.60 mol·L(−1) FeCl(3) have the best absorption properties. The maximum value of reflection loss (RL) at 3 mm thickness reaches −25.60 dB at 10.16 GHz and the bandwidth below −10 dB is about 2.5 GHz. Compared to woodceramic, the bending strength and compressive strength of α-Fe/Fe(3)C/woodceramic nanocomposites increase by 22.5% and 18.7% at most, respectively. |
format | Online Article Text |
id | pubmed-6024902 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2018 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-60249022018-07-09 Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties Zhou, Weihong Yu, Yunshui Xiong, Xueliang Zhou, Sicong Materials (Basel) Article Furan resin and fir powder pretreated by FeCl(3) and aqueous ammonia solution were used to fabricate α-Fe/Fe(3)C/woodceramic nanocomposite. The bands of the pretreated wood powder were characterized by Fourier transform infrared spectroscopy (FTIR). The structural characterization of the nanocomposites was performed by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The microwave absorption of the nanocomposites was measured by a vector network analyzer in the range of 2–18 GHz. The mechanical properties of the composites were also investigated. XRD and SEM results show that the α-Fe and Fe(3)C nanoparticles are in-situ generated and disperse in the matrix of the woodceramic. The diameters of these nanoparticles increase with the increasing of concentration of FeCl(3) solution. The experimental results show that both the complex permittivity and the complex permeability of α-Fe/Fe(3)C/woodceramic nanocomposites increase as the concentration of FeCl(3) solution increases. The composites pretreated with 0.60 mol·L(−1) FeCl(3) have the best absorption properties. The maximum value of reflection loss (RL) at 3 mm thickness reaches −25.60 dB at 10.16 GHz and the bandwidth below −10 dB is about 2.5 GHz. Compared to woodceramic, the bending strength and compressive strength of α-Fe/Fe(3)C/woodceramic nanocomposites increase by 22.5% and 18.7% at most, respectively. MDPI 2018-05-24 /pmc/articles/PMC6024902/ /pubmed/29794971 http://dx.doi.org/10.3390/ma11060878 Text en © 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Zhou, Weihong Yu, Yunshui Xiong, Xueliang Zhou, Sicong Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties |
title | Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties |
title_full | Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties |
title_fullStr | Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties |
title_full_unstemmed | Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties |
title_short | Fabrication of α-Fe/Fe(3)C/Woodceramic Nanocomposite with Its Improved Microwave Absorption and Mechanical Properties |
title_sort | fabrication of α-fe/fe(3)c/woodceramic nanocomposite with its improved microwave absorption and mechanical properties |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6024902/ https://www.ncbi.nlm.nih.gov/pubmed/29794971 http://dx.doi.org/10.3390/ma11060878 |
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