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Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging

Specimen and stage drift as well as scan distortions can lead to a mismatch between true and desired electron probe positions in scanning transmission electron microscopy (STEM) which can result in both linear and nonlinear distortions in the subsequent experimental images. This problem is intensifi...

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Autores principales: Wang, Yi, Suyolcu, Y Eren, Salzberger, Ute, Hahn, Kersten, Srot, Vesna, Sigle, Wilfried, van Aken, Peter A
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Oxford University Press 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6025237/
https://www.ncbi.nlm.nih.gov/pubmed/29385502
http://dx.doi.org/10.1093/jmicro/dfy002
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author Wang, Yi
Suyolcu, Y Eren
Salzberger, Ute
Hahn, Kersten
Srot, Vesna
Sigle, Wilfried
van Aken, Peter A
author_facet Wang, Yi
Suyolcu, Y Eren
Salzberger, Ute
Hahn, Kersten
Srot, Vesna
Sigle, Wilfried
van Aken, Peter A
author_sort Wang, Yi
collection PubMed
description Specimen and stage drift as well as scan distortions can lead to a mismatch between true and desired electron probe positions in scanning transmission electron microscopy (STEM) which can result in both linear and nonlinear distortions in the subsequent experimental images. This problem is intensified in STEM spectrum and diffraction imaging techniques owing to the extended dwell times (pixel exposure time) as compared to conventional STEM imaging. As a consequence, these image distortions become more severe in STEM spectrum/diffraction imaging. This becomes visible as expansion, compression and/or shearing of the crystal lattice, and can even prohibit atomic resolution and thus limits the interpretability of the results. Here, we report a software tool for post-correcting the linear and nonlinear image distortions of atomically resolved 3D spectrum imaging as well as 4D diffraction imaging. This tool improves the interpretability of distorted STEM spectrum/diffraction imaging data.
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spelling pubmed-60252372018-07-10 Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging Wang, Yi Suyolcu, Y Eren Salzberger, Ute Hahn, Kersten Srot, Vesna Sigle, Wilfried van Aken, Peter A Microscopy (Oxf) Article Specimen and stage drift as well as scan distortions can lead to a mismatch between true and desired electron probe positions in scanning transmission electron microscopy (STEM) which can result in both linear and nonlinear distortions in the subsequent experimental images. This problem is intensified in STEM spectrum and diffraction imaging techniques owing to the extended dwell times (pixel exposure time) as compared to conventional STEM imaging. As a consequence, these image distortions become more severe in STEM spectrum/diffraction imaging. This becomes visible as expansion, compression and/or shearing of the crystal lattice, and can even prohibit atomic resolution and thus limits the interpretability of the results. Here, we report a software tool for post-correcting the linear and nonlinear image distortions of atomically resolved 3D spectrum imaging as well as 4D diffraction imaging. This tool improves the interpretability of distorted STEM spectrum/diffraction imaging data. Oxford University Press 2018-03 2018-01-29 /pmc/articles/PMC6025237/ /pubmed/29385502 http://dx.doi.org/10.1093/jmicro/dfy002 Text en © The Author(s) 2018. Published by Oxford University Press on behalf of The Japanese Society of Microscopy. http://creativecommons.org/licenses/by-nc/4.0/ This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/4.0/), which permits non-commercial re-use, distribution, and reproduction in any medium, provided the original work is properly cited. For commercial re-use, please contact journals.permissions@oup.com
spellingShingle Article
Wang, Yi
Suyolcu, Y Eren
Salzberger, Ute
Hahn, Kersten
Srot, Vesna
Sigle, Wilfried
van Aken, Peter A
Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging
title Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging
title_full Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging
title_fullStr Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging
title_full_unstemmed Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging
title_short Correcting the linear and nonlinear distortions for atomically resolved STEM spectrum and diffraction imaging
title_sort correcting the linear and nonlinear distortions for atomically resolved stem spectrum and diffraction imaging
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6025237/
https://www.ncbi.nlm.nih.gov/pubmed/29385502
http://dx.doi.org/10.1093/jmicro/dfy002
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