Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one

In the title compound, C(18)H(19)NO(3)S, the morpholine ring adopts a chair conformation. The thio­phene ring forms dihedral angles of 26.04 (9) and 74.07 (10)° with the benzene ring and the mean plane of the morpholine ring, respectively. The mol­ecular conformation is stabilized by an O—H⋯N hydrog...

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Autores principales: Yesilyurt, Fatma, Aydin, Abdullah, Gul, Halise Inci, Akkurt, Mehmet, Ozcelik, Nefise Dilek
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2018
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6038634/
https://www.ncbi.nlm.nih.gov/pubmed/30002894
http://dx.doi.org/10.1107/S2056989018008459
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author Yesilyurt, Fatma
Aydin, Abdullah
Gul, Halise Inci
Akkurt, Mehmet
Ozcelik, Nefise Dilek
author_facet Yesilyurt, Fatma
Aydin, Abdullah
Gul, Halise Inci
Akkurt, Mehmet
Ozcelik, Nefise Dilek
author_sort Yesilyurt, Fatma
collection PubMed
description In the title compound, C(18)H(19)NO(3)S, the morpholine ring adopts a chair conformation. The thio­phene ring forms dihedral angles of 26.04 (9) and 74.07 (10)° with the benzene ring and the mean plane of the morpholine ring, respectively. The mol­ecular conformation is stabilized by an O—H⋯N hydrogen bond. In the crystal, mol­ecules are connected through C—H⋯O hydrogen bonds, forming wave-like layers parallel to the ab plane, which are further linked into a three-dimensional network by C—H⋯π inter­actions involving the benzene rings and the methyl­ene H atoms of the morpholine rings.
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spelling pubmed-60386342018-07-12 Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one Yesilyurt, Fatma Aydin, Abdullah Gul, Halise Inci Akkurt, Mehmet Ozcelik, Nefise Dilek Acta Crystallogr E Crystallogr Commun Research Communications In the title compound, C(18)H(19)NO(3)S, the morpholine ring adopts a chair conformation. The thio­phene ring forms dihedral angles of 26.04 (9) and 74.07 (10)° with the benzene ring and the mean plane of the morpholine ring, respectively. The mol­ecular conformation is stabilized by an O—H⋯N hydrogen bond. In the crystal, mol­ecules are connected through C—H⋯O hydrogen bonds, forming wave-like layers parallel to the ab plane, which are further linked into a three-dimensional network by C—H⋯π inter­actions involving the benzene rings and the methyl­ene H atoms of the morpholine rings. International Union of Crystallography 2018-06-12 /pmc/articles/PMC6038634/ /pubmed/30002894 http://dx.doi.org/10.1107/S2056989018008459 Text en © Yesilyurt et al. 2018 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/2.0/uk/
spellingShingle Research Communications
Yesilyurt, Fatma
Aydin, Abdullah
Gul, Halise Inci
Akkurt, Mehmet
Ozcelik, Nefise Dilek
Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
title Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
title_full Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
title_fullStr Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
title_full_unstemmed Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
title_short Crystal structure and theoretical study of (2E)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
title_sort crystal structure and theoretical study of (2e)-1-[4-hy­droxy-3-(morpholin-4-ylmeth­yl)phen­yl]-3-(thio­phen-2-yl)prop-2-en-1-one
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6038634/
https://www.ncbi.nlm.nih.gov/pubmed/30002894
http://dx.doi.org/10.1107/S2056989018008459
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