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Toroidal diamond anvil cell for detailed measurements under extreme static pressures

Over the past 60 years, the diamond anvil cell (DAC) has been developed into a widespread high static pressure device. The adaptation of laboratory and synchrotron analytical techniques to DAC enables a detailed exploration in the 100 GPa range. The strain of the anvils under high load explains the...

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Autores principales: Dewaele, Agnès, Loubeyre, Paul, Occelli, Florent, Marie, Olivier, Mezouar, Mohamed
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6060175/
https://www.ncbi.nlm.nih.gov/pubmed/30046093
http://dx.doi.org/10.1038/s41467-018-05294-2
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author Dewaele, Agnès
Loubeyre, Paul
Occelli, Florent
Marie, Olivier
Mezouar, Mohamed
author_facet Dewaele, Agnès
Loubeyre, Paul
Occelli, Florent
Marie, Olivier
Mezouar, Mohamed
author_sort Dewaele, Agnès
collection PubMed
description Over the past 60 years, the diamond anvil cell (DAC) has been developed into a widespread high static pressure device. The adaptation of laboratory and synchrotron analytical techniques to DAC enables a detailed exploration in the 100 GPa range. The strain of the anvils under high load explains the 400 GPa limit of the conventional DAC. Here we show a toroidal shape for a diamond anvil tip that enables to extend the DAC use toward the terapascal pressure range. The toroidal-DAC keeps the assets for a complete, reproducible, and accurate characterization of materials, from solids to gases. Raman signal from the diamond anvil or X-ray signal from the rhenium gasket allow measurement of pressure. Here, the equations of state of gold, aluminum, and argon are measured with X-ray diffraction. The data are compared with recent measurements under similar conditions by two other approaches, the double-stage DAC and the dynamic ramp compression.
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spelling pubmed-60601752018-07-27 Toroidal diamond anvil cell for detailed measurements under extreme static pressures Dewaele, Agnès Loubeyre, Paul Occelli, Florent Marie, Olivier Mezouar, Mohamed Nat Commun Article Over the past 60 years, the diamond anvil cell (DAC) has been developed into a widespread high static pressure device. The adaptation of laboratory and synchrotron analytical techniques to DAC enables a detailed exploration in the 100 GPa range. The strain of the anvils under high load explains the 400 GPa limit of the conventional DAC. Here we show a toroidal shape for a diamond anvil tip that enables to extend the DAC use toward the terapascal pressure range. The toroidal-DAC keeps the assets for a complete, reproducible, and accurate characterization of materials, from solids to gases. Raman signal from the diamond anvil or X-ray signal from the rhenium gasket allow measurement of pressure. Here, the equations of state of gold, aluminum, and argon are measured with X-ray diffraction. The data are compared with recent measurements under similar conditions by two other approaches, the double-stage DAC and the dynamic ramp compression. Nature Publishing Group UK 2018-07-25 /pmc/articles/PMC6060175/ /pubmed/30046093 http://dx.doi.org/10.1038/s41467-018-05294-2 Text en © The Author(s) 2018 Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.
spellingShingle Article
Dewaele, Agnès
Loubeyre, Paul
Occelli, Florent
Marie, Olivier
Mezouar, Mohamed
Toroidal diamond anvil cell for detailed measurements under extreme static pressures
title Toroidal diamond anvil cell for detailed measurements under extreme static pressures
title_full Toroidal diamond anvil cell for detailed measurements under extreme static pressures
title_fullStr Toroidal diamond anvil cell for detailed measurements under extreme static pressures
title_full_unstemmed Toroidal diamond anvil cell for detailed measurements under extreme static pressures
title_short Toroidal diamond anvil cell for detailed measurements under extreme static pressures
title_sort toroidal diamond anvil cell for detailed measurements under extreme static pressures
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6060175/
https://www.ncbi.nlm.nih.gov/pubmed/30046093
http://dx.doi.org/10.1038/s41467-018-05294-2
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