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Synthesis of Thieno[2,3-d]-1,3-dithiol-2-thiones from Thieno[2,3-d]-1,2,3-thiadiazoles: Matryoshka-type autoclave for high-temperature, high-pressure thermolysis microscale reactions†

Thieno[2,3-d]-1,2,3-thiadiazoles (1) react with carbon disulfide in a "Matryoshka-type" double compartment autoclave [1] to yield thieno[2,3-d]-1,3-dithiol-2-thiones (2). With BH(3)/Me(2)S the cyclic trithiocarbonate (2d) is cleaved and the product characterized after methylation as 4b. Co...

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Detalles Bibliográficos
Autores principales:	Jordis, Ulrich, Bhattacharya, Kaberi, Boamah, Philip Y., Lee, Ving J.
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	MDPI 2002
Materias:	Article
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146433/ http://dx.doi.org/10.3390/70200145

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