Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†

Easy and effective preparations of nearly pure (diacetoxyiodo)arenes, ArI(OAc)(2), from iodoarenes, ArI, are reported. In most cases the crude colorless products thus obtained need not be further purified, i.e., by recrystallization. As an example, the PhI(OAc)(2) thus prepared was 99% pure (by iodo...

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Detalles Bibliográficos
Autores principales: Zielinska, Agnieszka, Skulski, Lech
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2002
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146435/
http://dx.doi.org/10.3390/71100806
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author Zielinska, Agnieszka
Skulski, Lech
author_facet Zielinska, Agnieszka
Skulski, Lech
author_sort Zielinska, Agnieszka
collection PubMed
description Easy and effective preparations of nearly pure (diacetoxyiodo)arenes, ArI(OAc)(2), from iodoarenes, ArI, are reported. In most cases the crude colorless products thus obtained need not be further purified, i.e., by recrystallization. As an example, the PhI(OAc)(2) thus prepared was 99% pure (by iodometry).
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spelling pubmed-61464352018-11-19 Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant† Zielinska, Agnieszka Skulski, Lech Molecules Article Easy and effective preparations of nearly pure (diacetoxyiodo)arenes, ArI(OAc)(2), from iodoarenes, ArI, are reported. In most cases the crude colorless products thus obtained need not be further purified, i.e., by recrystallization. As an example, the PhI(OAc)(2) thus prepared was 99% pure (by iodometry). MDPI 2002-11-30 /pmc/articles/PMC6146435/ http://dx.doi.org/10.3390/71100806 Text en © 2002 by MDPI (http://www.mdpi.org). Reproduction is permitted for noncommercial purposes.
spellingShingle Article
Zielinska, Agnieszka
Skulski, Lech
Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†
title Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†
title_full Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†
title_fullStr Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†
title_full_unstemmed Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†
title_short Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant†
title_sort easy preparation of (diacetoxyiodo)arenes from iodoarenes with sodium percarbonate as the oxidant†
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146435/
http://dx.doi.org/10.3390/71100806
work_keys_str_mv AT zielinskaagnieszka easypreparationofdiacetoxyiodoarenesfromiodoareneswithsodiumpercarbonateastheoxidant
AT skulskilech easypreparationofdiacetoxyiodoarenesfromiodoareneswithsodiumpercarbonateastheoxidant

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