Cargando…
Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one
The synthesis of a new spirolactone is described. The title compound is obtained as a white solid in 46% yield from 3-(4-hydroxy-2-methoxyphenyl)propanoic acid using [Bis(trifluoroacetoxy)iodo]benzene (PIFA) as the oxidant.
| Autores principales: | , |
|---|---|
| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
MDPI
2002
|
| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146477/ http://dx.doi.org/10.3390/70200315 |
| _version_ | 1783356402337579008 |
|---|---|
| author | Plourde, Guy L. Fisher, Benjamin B. |
| author_facet | Plourde, Guy L. Fisher, Benjamin B. |
| author_sort | Plourde, Guy L. |
| collection | PubMed |
| description | The synthesis of a new spirolactone is described. The title compound is obtained as a white solid in 46% yield from 3-(4-hydroxy-2-methoxyphenyl)propanoic acid using [Bis(trifluoroacetoxy)iodo]benzene (PIFA) as the oxidant. |
| format | Online Article Text |
| id | pubmed-6146477 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2002 |
| publisher | MDPI |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-61464772018-11-19 Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one Plourde, Guy L. Fisher, Benjamin B. Molecules Article The synthesis of a new spirolactone is described. The title compound is obtained as a white solid in 46% yield from 3-(4-hydroxy-2-methoxyphenyl)propanoic acid using [Bis(trifluoroacetoxy)iodo]benzene (PIFA) as the oxidant. MDPI 2002-02-28 /pmc/articles/PMC6146477/ http://dx.doi.org/10.3390/70200315 Text en © 2002 by MDPI (http://www.mdpi.org). Reproduction is permitted for non commercial purposes. |
| spellingShingle | Article Plourde, Guy L. Fisher, Benjamin B. Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| title | Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| title_full | Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| title_fullStr | Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| title_full_unstemmed | Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| title_short | Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| title_sort | synthesis of 6-methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one |
| topic | Article |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146477/ http://dx.doi.org/10.3390/70200315 |
| work_keys_str_mv | AT plourdeguyl synthesisof6methoxy1oxaspiro45deca69diene8one AT fisherbenjaminb synthesisof6methoxy1oxaspiro45deca69diene8one |